438624-68-1Relevant articles and documents
Synthesis of 3H, 14C and 13C6 labelled Sch 58235
Hesk,Bignan,Lee,Yang,Voronin,Magatti,McNamara,Koharski,Hendershot,Saluja,Wang
, p. 145 - 155 (2007/10/03)
3H-Sch 58235 was prepared at a specific activity of 29.1 Ci/mmol by Ir(COD)(Cy3P)PyPF6 catalysed exchange with tritium gas. 14C-Sch 58235 was prepared in three steps from p-hydroxy[ring-U-14C]benzaldehyde with an overall radiochemical yield of 21%. 13C6-Sch 58235 was similarly prepared in three steps from p-hydroxy[ring-U-13C6]benzaldehyde in an overall yield of 41%. Copyright