4819-82-3Relevant articles and documents
Synthesis of sulfonic acid functionalized carbon catalyst from glycerol pitch and its application for tetrahydropyranyl protection/deprotection of alcohols and phenols
Prabhavathi Devi,Gangadhar,Siva Kumar,Shiva Shanker,Prasad,Sai Prasad
experimental part, p. 96 - 100 (2011/10/05)
A novel carbon catalyst with -SO3H, -OH and -COOH functional groups was prepared from glycerol pitch by in situ partial carbonization and sulfonation with sulfuric acid. The activity of the catalyst was investigated through tetrahydropyranylation and dehydropyranylation of a wide variety of alcohols and phenols at room temperature by changing the solvent medium from dichloromethane to methanol. Excellent yields, short reaction times, easy and quick isolation of the products and reusability of the catalyst are the main attractions of this method. The novel carbon catalyst holds great potential in the green chemical processes.
The use of basic resin in the preparation of tetrahydropyranyl derivatives of alcohols and phenols
Chaturvedi, Devdutt,Kumar, Atul,Ray
, p. 437 - 438 (2007/10/03)
A quick and efficient method for the preparation of tetrahydropyranyl (THP) derivatives of phenols and alcohols using a basic resin IRA-400 (iodide) is described.
Solvent-Free Tetrahydropyranylation of Alcohols with Sulfamic Acid as Reusable Catalyst
Wang, Bo,Yang, Li-Ming,Suo, Ji-Shuan
, p. 3929 - 3934 (2007/10/03)
An efficient H2NSO3H-catalyzed solvent-free tetrahydropyranylation of various alcohols at room temperature was investigated. The features of mild conditions, cost-efficient catalyst, simple work-up, and the recyclability of the catalyst were displayed in this article.