cas 604799-99-7, (E)-1-STYRYLCYCLOPROPANAMINE | Articles data ｜lookchem

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604799-99-7

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A direct synthesis of 1-aryl- and 1-alkenylcyclopropylamines from aryl and alkenyl nitriles
The reaction of various aromatic nitriles with 1.1 equiv of Ti(Oi-Pr)4 and 2.2 equiv of EtMgBr followed by addition of a Lewis acid gave 1-aryl cyclopropylamines in 43-76% yields. Under similar conditions, conjugated alkene-nitriles afford 1-alkenylcyclopropylamines (42-65%).
Bertus, Philippe,Szymoniak, Jan
p. 7133 - 7136
(2007/10/03)

Regioselective palladium (0) catalyzed azidation and amination of 1-alkenylcyclopropyl esters: A new route to 2,3-methanoamino acids
Palladium (0) catalyzed azidation of 1-alkenylcyclopropyl esters provides regioselectively 1-azido-1-alkenyl cyclopropanes, convenient precursors of 2,3-methanoamino acids. On the other hand, amination occurred exclusively on the less substituted allylic end, providing strained 2-cyclopropylideneethylamine derivatives.
Aufranc,Ollivier,Stolle,Bremer,Es-Sayed,De Meijere,Salaun
p. 4193 - 4196
(2007/10/02)

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152449-89-3
[1-((E)-Styryl)-cyclopropyl]-carbamic acid tert-butyl ester

Chemical Properties

Boiling Point: 253.7±19.0 °C(Predicted)
Density: 1.159±0.06 g/cm3(Predicted)
PKA: 8.46±0.20(Predicted)
PSA: 26.02000
LogP: 2.89140

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