cas 63930-59-6, 3-oxocyclobutyl acetate | Articles data

3-Acetoxycyclobutanone is a versatile intermediate to access cyclobutanes with a variety of substitution patterns. Established procedures require a two step process that includes multiple distillations. We report a one-pot procedure that renders this compound readily available. Additionally, it was determined that copper plays a key role in the reaction sequence.

3-Substituted cyclobutanones 2 are prepared by alkene/dichloroketene cycloadditions and subsequent dehalogenation.Reduction with LiAlH(OtBu)3 furnishes cis-cyclobutanols 3 in 95-100percent selectivity.Mitsunobu inversion turned out to be the only practica

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Chemical Properties

Boiling Point: 188.0±33.0 °C(Predicted)

Density: 1.16±0.1 g/cm3(Predicted)

Storage Temp.:2-8°C

PSA: 43.37000

LogP: 0.28100

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