cas 64473-34-3, 3-(4'-CHLOROPHENYL)PROPYL CHLORIDE | Articles data ｜lookchem

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64473-34-3

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Room temperature C(sp2)-H oxidative chlorination: Via photoredox catalysis
Photoredox catalysis has been developed to achieve oxidative C-H chlorination of aromatic compounds using NaCl as the chlorine source and Na2S2O8 as the oxidant. The reactions occur at room temperature and exhibit exclusive selectivity for C(sp2)-H bonds over C(sp3)-H bonds. The method has been used for the chlorination of a diverse set of substrates, including the expedited synthesis of key intermediates to bioactive compounds and a drug.
Zhang, Lei,Hu, Xile
p. 7009 - 7013
(2017/10/05)

Cobalt-catalyzed ortho alkylation of aromatic imines with primary and secondary alkyl halides
We report here cobalt-N-heterocyclic carbene catalytic systems for the ortho alkylation of aromatic imines with alkyl chlorides and bromides, which allows the introduction of a variety of primary and secondary alkyl groups at room temperature. The stereochemical outcomes of the reaction of secondary alkyl halides suggest that the present reaction involves single-electron transfer from a cobalt species to the alkyl halide to generate the corresponding alkyl radical. A cycloalkylated product obtained by this method can be transformed into unique spirocycles through manipulation of the directing and cycloalkyl groups.
Gao, Ke,Yoshikai, Naohiko
supporting information
p. 9279 - 9282
(2013/07/19)

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Chemical Properties

Melting Point: 0°C
Boiling Point: 254.9 °C at 760 mmHg
Flash Point:104.5 °C
Density: 1.166 g/cm³
Vapor Pressure: 0.027mmHg at 25°C
Refractive Index: 1.531
PSA: 0.00000
LogP: 3.51140

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