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6485-58-1

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Mechanistic Investigation of Carbon-Carbon Bond Formation in the Reduction of Alkyl Halides by Organonickel Complexes in Aqueous Solution
The macrocyclic alkylnickel(II) complexes, RNi(tmc)+ (R = C2H5, C3H7, and CH2-c-C5H9; tmc = (1R,4R,8S,11S)-1,4,8,11-tetramethyl-1,4,8.11-tetraazacyclotetradecane), react with alkyl halides R'X (R'= CH3, C2H5, 1-C3H7, 2-C3H7, and PhCH2) in alkaline aqueous solutions, yielding combination and disproportionation products of R and R'.The reactivity of R'X increases in the order methyl . + 2-C3H7I -> 2-C3H7. + C2H5I in aqueous solution was determined by competition with V(H2O)62+.The value k2-PrI ca. 6E5 M-1s-1 is significantly higher than in aprotic solvents.
Bakac, Andreja,Espenson, James H.
p. 719 - 723
(2007/10/02)

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Chemical Properties

Appearance/Colour :clear colorless liquid
Melting Point: -108 °C(lit.)
Boiling Point: 69-73 °C(lit.)
Flash Point:53 °C
Density: 2.012 g/mL at 25 °C
Solubility:Chloroform, Ethyl Acetate
Storage Temp.:Flammables area
Vapor Pressure: 128mmHg at 25°C
Refractive Index: n20/D 1.5091(lit.)
BRN: 1840101
PSA: 0.00000
LogP: 1.44130

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