The synthesis of [3H] and [14C]o- chlorobenzylidenemalononitrile (CS)
Using similar procedures, the syntheses of [2-14C]-malononitrile and malono [14C]nitrile are described. Condensation with o-chlorobenzaldehyde affords [2-14C]-o-chlorobenzylidenemalononitrile and o-chlorobenzylidenemalono [14C]nitrile respectively. The syntheses of [3H]o-chlorobenzaldehyde and o-chlorobenz[ 14C]aldehyde, again by a common sequence of reactions, is described and with malononitrile gives [3H]-o-chlorobenzylidenemalononitrile and [1-14C]-o-chlorobenzylidenemalononitrile.
Harrison,Inch,Lawston,Ley,Sainsbury
p. 141 - 148
(2014/02/14)
Synthesis of C14-labeled guanine, adenine, 8-azaguanine and 8-azaadenine
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Bennett, Edward L.
p. 2420 - 2422
(2014/01/06)
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