cas 67707-85-1, 1,4,8,11-Tetraazacyclotetradecane, 1,4,8-trimethyl- | Articles data ｜lookchem

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67707-85-1

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Efficient preparation of 1,4,8-trimethylcyclam and its conversion into a thioalkyl-pendant pentadentate chelate
A facile synthesis of 1,4,8-trimethylcyclam and a thioalkyl-pendant derivative are reported, and the X-ray crystal structure of a nickel(II) complex illustrates structural consequences of appending the thiolate donor onto the macrocycle.
Halfen, Jason A.,Young Jr., Victor G.
p. 2894 - 2895
(2007/10/03)

New high yield syntheses of cyclams using the crab-like cyclization reaction
A new high yield method to synthesize cyclams containing one or two unsubstituted ring nitrogen atoms and with alkyl groups on the remaining ring nitrogen atoms is presented. The method consists of the ring closure reaction of a crab-like bis-α-chloroamide with a bis-secondary amine followed by reduction. The amide functions of the starting material act as protecting groups for the protons on the amide nitrogen atoms.
Bradshaw,Krakowiak,Izatt,Zamecka-Krakowiak
p. 1077 - 1080
(2007/10/02)

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Chemical Properties

Boiling Point: 306.6°C at 760 mmHg
Flash Point:123.5°C
Density: 0.873g/cm³
Vapor Pressure: 0.000764mmHg at 25°C
PSA: 21.75000
LogP: 0.30770

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