- Ionic liquid-induced conversion of methoxymethyl-protected alcohols into nitriles and iodides using [Hmim][NO3]
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This Letter reports a one-pot efficient conversion of methoxymethyl-ethers into their corresponding nitriles and iodides using the ionic liquid, 1-methyl-3H-imidazolium nitrate ([Hmim][NO3]) under microwave irradiation. A variety of products were prepared in high yields using this method.
- Noei, Jalil,Mirjafari, Arsalan
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supporting information
p. 4424 - 4426
(2014/08/05)
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- Efficient and selective iodination of benzylic alcohols using NaI/bronsted ionic liquid system at room temperature
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A simple, chemoselective, and effective procedure for the conversion of benzylic and allylic alcohols into corresponding iodides using NaI in the presence of a catalytic amount of 3-methylimidazolium hydrogensulfate ([Hmim]+[image omitted]) at room temperature is reported.
- Hajipour, Abdol R.,Rafiee, Fatemeh,Ruoho, Arnold
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experimental part
p. 603 - 611
(2011/04/15)
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- Microwave-promoted, one-pot conversion of alkoxymethylated protected alcohols into their corresponding nitriles, bromides, and iodides using [bmim][InCl4] as a green catalyst
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The Lewis acid room temperature ionic liquid, [bmim][InCl4], was found to be an efficient and green catalyst for the highly chemoselective and one-pot conversion of MOM- or EOM-ethers into their corresponding nitriles, bromides, and iodides under microwave irradiation. The procedures are simple, rapid, and high yielding. The catalyst exhibited a remarkable reactivity and is reusable.
- Mirjafari, Arsalan,Mohammadpoor-Baltork, Iraj,Moghadam, Majid,Tangestaninejad, Shahram,Mirkhani, Valiollah,Khosropour, Ahmad Reza
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supporting information; experimental part
p. 3274 - 3276
(2010/07/18)
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- Iodination of alcohols under microwave irradiation using KI in the presence of a catalytic amount of ionic liquid triethylamoniom hydrogensulfate([Et 3NH]+HSO4-)
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The iodination of alcohols with KI in the presence of a catalytic amount of triethylamoniom hydrogensulfate ([Et3NH]+HSO 4-) as a novel and inexpensive ionic liquid under microwave irradiation has been investigated. Copyright Taylor & Francis Group, LLC.
- Hajipour, Abdol R.,Azizi, Ghobad,Ruoho, Arnold E.
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experimental part
p. 242 - 250
(2009/04/07)
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- Solvent-free conversion of alcohols into iodides with NaI supported on KSF clay
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A variety of allylic, benzylic, primary, and secondary saturated alcohols have been converted into the corresponding iodides using NaI supported on KSF clay. Selective conversion of allylic and benzylic alcohols in the presence of primary and secondary saturated alcohols has also been demonstrated. Copyright Taylor & Francis, Inc.
- Tajbakhsh, Mahmood,Hosseinzadeh, Rahman,Lasemi, Zahra,Rostami, Ali
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p. 2905 - 2911
(2007/10/03)
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- Selective iodination of alcohols with NaI/Amberlyst 15 in acetonitrile
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A simple and effective procedure for conversion of primary, secondary, allylic and benzylic alcohols into the corresponding iodides is described using NaI/Amberlyst 15 in acetonitrile at room temperature. Selective conversion of benzylic alcohols in the presence of saturated alcohols into the corresponding benzylic iodides is achieved under these conditions.
- Tajbakhsh, Mahmood,Hosseinzadeh, Rahman,Lasemi, Zahra
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p. 635 - 638
(2007/10/03)
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