- Method for TORTNB etherification synthesis in microreactor
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The invention discloses a method for TORTNB etherification synthesis in microreactor. The method includes steps: dissolving a nitrification product TNPG into an organic solvent; simultaneously pumpingTNPG solution and an etherification into a micro mixer,
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Paragraph 0021; 0022; 0025-0032
(2019/04/06)
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- METHODS OF PRODUCING 1,3,5-TRIAMINO-2,4,6-TRINITROBENZENE
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Methods of producing TATB are disclosed. The method comprises providing acid wet TNPG and distilling water from the acid wet TNPG. The TNPG is reacted with an alkoxylating agent to form a solution of 1,3,5-trialkoxy-2,4,6-trinitrobenzene solution, which is reacted with an aminating agent. An alternate method comprises nitrating phloroglucinol in a first vessel to produce TNPG, which is reacted with an alkoxylating agent in a second vessel to form a solution comprising 1,3,5-trialkoxy-2,4,6-trinitrobenzene and at least one of at least one volatile byproduct and at least one nonvolatile byproduct. The at least one of at least one volatile byproduct and at least one nonvolatile byproduct is removed in situ. The 1,3,5-trialkoxy-2,4,6-trinitrobenzene is reacted with an aminating agent.
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