Hydration of Diacetylene Compounds. Synthesis of a Marine Natural Product: (+/-)-1-(2,6,6-Trimethyl-4-hydroxycyclohexenyl)-1,3-butanedione
The marine natural product (+/-)-1-(2,6,6-trimethyl-4-hydroxycyclohexenyl)-1,3-butanedione (1) was synthesized from known the keto alcohol 3 and 1,4-dichlorobut-2-yne.The synthetic sequence involves dehydration of the diyne tertiary alcohol 2 and hydratio
Constantino, Mauricio G.,Donate, Paulo M.,Petragnani, Nicola
p. 387 - 390
(2007/10/02)
SYNTHESIS OF (+/-)-1-(2,6,6-TRIMETHYL-4-HYDROXYCYCLOHEXENYL)-1,3-BUTANEDIONE (1), A MARINE NATURAL PRODUCT
A short synthesis of racemic natural product (1) from the known compound (7) is described.A model study, using cyclohexanone as starting material, is also reported.
Constantino, Mauricio G.,Donate, Paulo M.,Petragnani, Nicola
p. 1051 - 1054
(2007/10/02)
Synthesis of 1-(2,6,6-Trimethyl-4-hydroxy-1-cyclohexen-1-yl)-1,3-butanedione
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Tsujino, Yasuko,Kaneko, Hajime
p. 2163 - 2164
(2007/10/02)
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