OLIGODEOXYRIBONUCLEOTIDE SYNTHESIS BY USE OF S,S-DIPHENYL DEOXYRIBONUCLEOSIDE 3'-PHOSPHORODITHIOATES AND BIFUNCTIONAL CONDENSING REAGENTS IN THE PHOSPHOTRIESTER APPROACH
Four kinds of arenedisulphonyl chlorides as condensing reagents for oligodeoxyribonucleotide synthesis have been synthesised and their condensing abilities were examined in the synthesis of thymidylyl(3'-5')thymidine.Among them, mesitylenedisulphonyl chlo
Sekine, Mitsuo,Matsuzaki, Jun-Ichi,Hata, Tsujiaki
p. 5279 - 5288
(2007/10/02)
PHOSPHOTRIESTER APPROACH TO OLIGOTHYMIDYLATE SYNTHESIS UTILIZING A SIMPLE THYMIDINE UNIT AND A NEW TYPE OF CONDENSING AGENT
DMTrTp(SPh)2 was proposed as a simplest "nucleotide unit" for the synthesis of olygothymidylates.One phenylthio group was removed selectively and rapidly from dithiol-esters by 1M pyridinium hypophosphonate.Two kinds of arenedisulfonyl chlorides were newl
Sekine, Mitsuo,Matsuzaki, Jun-ichi,Hata, Tsujiaki
p. 3209 - 3212
(2007/10/02)
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