Preparative chromatography with extreme productivity: HPLC preparation of an isomerically pure drug intermediate on multikilogram scale
A highly productive method for HPLC preparation of 7.5 kg of an isomerically pure drug intermediate is described. The method employs an IPA/heptane eluent with a Chromegabond Nitro stationary phase, and affords an unusually large productivity of 5.5 kkd (
Welch, Christopher J.,Henderson, Derek W.,Tschaen, David M.,Miller, Ross A.
scheme or table
p. 621 - 624
(2010/04/22)
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