cas 85290-76-2, Ethyl 1,3-dimethyl-1H-pyrazole-4-carboxylate | Articles data ｜lookchem

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85290-76-2

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Process for the preparation of derivatives of 1-substituted-3-fluoroalkyl-pyrazole-4-carboxylic acid in the presence of ammonium salt
A process for the manufacture of a compound of the general formula (I) wherein - Y is H, F, an alkyl group, a cycloalkyl group, an aralkyl group or an aryl group, - R1 is H or an organic residue, - R2 is H or an organic residue ; which comprises submitting a compound of formula (II) wherein Y is as defined above, R1, is H or an organic residue, R2, is H or an organic residue, X is Cl, Br, I, CN, sulphate or sulphonate ; to a reduction reaction in the presence of an ammonium salt.
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Paragraph 0049; 0050

(2014/02/15)

A one-pot process for the regioselective synthesis of 1,3,4-trisubstituted-1H-pyrazoles
This Letter reports a facile and regioselective one-pot synthesis of 1,3,4-trisubstituted-1H-pyrazoles. It comprises a three-step telescoped sequence, which has been utilised in the production of a variety of differentially substituted pyrazoles.
Raw, Steven A.,Turner, Andrew T.
experimental part
p. 696 - 699
(2011/02/27)

Systemic fungicides. The synthesis of certain pyrazole analogues of carboxin
-
Huppatz
p. 135 - 147
(2007/10/02)

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103946-59-4
(1,3-dimethyl-1H-pyrazol-4-yl)methanol

Chemical Properties

Melting Point: 58-59 °C
Boiling Point: 85-86 °C(Press: 0.1 Torr)
Density: 1.12±0.1 g/cm3(Predicted)
PKA: 0.58±0.10(Predicted)
PSA: 44.12000
LogP: 0.90520

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