86522-86-3Relevant articles and documents
Preparation method of 4-halogenated-3-fluorotoluene
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Paragraph 0065-0066, (2021/03/31)
The invention belongs to the field of organic synthesis, and particularly relates to a preparation method of 4-halogenated -3-fluorotoluene. The preparation reaction of 4-halogenated -3-fluorotolueneshown as a formula (I) is shown in the specification. According to the method, halogenation reaction is conducted on 3-fluorotoluene serving as an initial raw material to obtain a halide, and hydrogenreduction is conducted to obtain a compound shown in the general formula (I), wherein X is chlorine or bromine. According to the method, 3-fluorotoluene is used as a raw material, and a target product is obtained through two-step reactions of halogenation and reduction. The reaction steps in the process are few; diazotization, nitrification and other reactions are avoided, and the reaction safetyis high.
Process for preparing 4,5-difluorobenzaldehydes
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, (2008/06/13)
4,5-Difluorobenzaldehydes of a given formula are prepared by the reaction of corresponding benzaldehydes with a fluorinating agent.
2,4-Dichloro-5-fluorobenzoyl halide and a process for its preparation
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, (2008/06/13)
The invention relates to 2,4-dichloro-r-fluorobenzoyl halide (particularly the chloride) and methods for its production. Also included in the invention are intermediates useful for the production of said 2,4-dichloro-5-fluorobenzoyl halide (particularly the chloride).