- Reaction of 1,1'-Iminobis-2-butanols with Sulfuric Acid
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Treatment of 1,1'-iminobis-2-butanols with 70percent w/w sulfuric acid gives cis- and trans-2,6-diethylmorpholines, 3-ethyl-4-methylpyridine and unsaturated 3-ethyl-4-methylpiperidines.Hydrogenation of the unsaturated 3-ethyl-4-methylpiperidines gives cis- and trans-3-ethyl-4-methylpiperidines.With 50percent w/w sulfuric acid cis- and trans-2,6-diethylmorpholines and a small amount of cis- and trans-2-ethyl-7-methyl-hexahydro-1,4-oyazepines are obtained
- Hernestam, Sven
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p. 1681 - 1685
(2007/10/02)
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