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Cas Database

100008-20-6

100008-20-6

Identification

  • Product Name:Boc-Pro-Gly-OPac

  • CAS Number: 100008-20-6

  • EINECS:

  • Molecular Weight:390.436

  • Molecular Formula:C20H26N2O6

  • HS Code:

  • Mol File:100008-20-6.mol

Synonyms:

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    Relevant articles and documentsAll total 2 Articles be found

    Optimization of the β-casomorphine-5 synthesis

    Hartrodt,Neubert,Matthies,et al.

    , p. 201 - 201 (2007/10/02)

    -

    An efficient method for the synthesis of phenacyl ester-protected dipeptides using neutral alumina-supported sodium carbonate 'Na2CO3/n-Al2O3'

    Hashimoto, Chikao,Sugimoto, Kazuhiro,Takahashi, Youhei,Kodomari, Mitsuo

    , p. 659 - 662 (2013/09/23)

    In the synthesis of dipeptides (Boc-AA1-AA2-OPac: AA1 and AA2 represent amino acids) protected by phenacyl (Pac) ester, amines and solid bases as the base for the conversion of the trifluoroacetic acid (TFA) sal

    Process route upstream and downstream products

    Process route

    1-(tert-butoxycarbonyl)-L-proline
    15761-39-4,59433-50-0

    1-(tert-butoxycarbonyl)-L-proline

    TFA·H-Gly-OPac

    TFA·H-Gly-OPac

    Boc-Pro-Gly-OPac
    100008-20-6

    Boc-Pro-Gly-OPac

    Conditions
    ConditionsYield
    With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;InN,N-dimethyl-formamide;at 0 - 20 ℃; for 24h; Reagent/catalyst;
    99 %Chromat.
    1-(tert-butoxycarbonyl)-L-proline
    15761-39-4,59433-50-0

    1-(tert-butoxycarbonyl)-L-proline

    glycine phenacyl ester
    83316-92-1

    glycine phenacyl ester

    Boc-Pro-Gly-OPac
    100008-20-6

    Boc-Pro-Gly-OPac

    Conditions
    ConditionsYield
    88%
    1-(tert-butoxycarbonyl)-L-proline
    15761-39-4,59433-50-0

    1-(tert-butoxycarbonyl)-L-proline

    TFA·H-Gly-OPac

    TFA·H-Gly-OPac

    Boc-Pro-Gly-OPac
    100008-20-6

    Boc-Pro-Gly-OPac

    Conditions
    ConditionsYield
    With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;InN,N-dimethyl-formamide;at 0 - 20 ℃; for 24h; Reagent/catalyst;
    99 %Chromat.
    1-(tert-butoxycarbonyl)-L-proline
    15761-39-4,59433-50-0

    1-(tert-butoxycarbonyl)-L-proline

    glycine phenacyl ester
    83316-92-1

    glycine phenacyl ester

    Boc-Pro-Gly-OPac
    100008-20-6

    Boc-Pro-Gly-OPac

    Conditions
    ConditionsYield
    88%

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