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Cas Database

100008-86-4

100008-86-4

Identification

  • Product Name:o-(β-ethoxycarbonylvinyl)phenyl N-phenylbenzohydrazidate

  • CAS Number: 100008-86-4

  • EINECS:

  • Molecular Weight:386.45

  • Molecular Formula: C24H22N2O3

  • HS Code:

  • Mol File:100008-86-4.mol

Synonyms:o-(β-ethoxycarbonylvinyl)phenyl N-phenylbenzohydrazidate

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Relevant articles and documentsAll total 1 Articles be found

Cycloaddition of diphenylnitrilimine to coumarins. The synthesis of 3a,9b-dihydro-4-oxo-1h-benzopyrano [4,3-c]pyrazole derivatives

Shawali,Elanadouli,Albar

, p. 1877 - 1884 (2007/10/02)

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Process route upstream and downstream products

Process route

(E)-ethyl 2-hydroxycinnamate
3943-94-0,17041-46-2,6236-62-0

(E)-ethyl 2-hydroxycinnamate

N-phenylbenzohydrazonoyl chloride
15424-14-3

N-phenylbenzohydrazonoyl chloride

o-(β-ethoxycarbonylvinyl)phenyl N-phenylbenzohydrazidate
100008-86-4

o-(β-ethoxycarbonylvinyl)phenyl N-phenylbenzohydrazidate

Conditions
Conditions Yield
With sodium ethanolate; In ethanol; 1.) reflux, 1 h; 2.) RT;
65%
ethanol
64-17-5

ethanol

coumarin
91-64-5

coumarin

N-phenylbenzohydrazonoyl chloride
15424-14-3

N-phenylbenzohydrazonoyl chloride

1,3,4,6-tetraphenyl-1,4-dihydro-1,2,4,5-tetrazine
17355-78-1

1,3,4,6-tetraphenyl-1,4-dihydro-1,2,4,5-tetrazine

o-(β-ethoxycarbonylvinyl)phenyl N-phenylbenzohydrazidate
100008-86-4

o-(β-ethoxycarbonylvinyl)phenyl N-phenylbenzohydrazidate

Conditions
Conditions Yield
With sodium ethanolate; for 3h; Heating;
55%
(E)-ethyl 2-hydroxycinnamate
3943-94-0,17041-46-2,6236-62-0

(E)-ethyl 2-hydroxycinnamate

N-phenylbenzohydrazonoyl chloride
15424-14-3

N-phenylbenzohydrazonoyl chloride

o-(β-ethoxycarbonylvinyl)phenyl N-phenylbenzohydrazidate
100008-86-4

o-(β-ethoxycarbonylvinyl)phenyl N-phenylbenzohydrazidate

Conditions
Conditions Yield
With sodium ethanolate; In ethanol; 1.) reflux, 1 h; 2.) RT;
65%
ethanol
64-17-5

ethanol

coumarin
91-64-5

coumarin

N-phenylbenzohydrazonoyl chloride
15424-14-3

N-phenylbenzohydrazonoyl chloride

1,3,4,6-tetraphenyl-1,4-dihydro-1,2,4,5-tetrazine
17355-78-1

1,3,4,6-tetraphenyl-1,4-dihydro-1,2,4,5-tetrazine

o-(β-ethoxycarbonylvinyl)phenyl N-phenylbenzohydrazidate
100008-86-4

o-(β-ethoxycarbonylvinyl)phenyl N-phenylbenzohydrazidate

Conditions
Conditions Yield
With sodium ethanolate; for 3h; Heating;
55%

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