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100008-93-3

100008-93-3

Identification

Synonyms:(2-methoxyphenyl)-2,4-dimethyl-5-nitropyridine

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Safety information and MSDS

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Relevant articles and documentsAll total 1 Articles be found

Synthesis of new pyrimidine derivatives from 2-methyl-3-nitro- and 3-amino-2-methylchromones

Tanaka,Murakami,Morita,Takagi

, p. 2129 - 2132 (2007/10/02)

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Process route upstream and downstream products

Process route

6-(2-hydroxyphenyl)-2,4-dimethyl-5-nitropyrimidine
100008-90-0

6-(2-hydroxyphenyl)-2,4-dimethyl-5-nitropyrimidine

methyl iodide
74-88-4

methyl iodide

(2-methoxyphenyl)-2,4-dimethyl-5-nitropyridine
100008-93-3

(2-methoxyphenyl)-2,4-dimethyl-5-nitropyridine

Conditions
Conditions Yield
With potassium hydroxide; In methanol; 1.) 1 h, reflux; 2.) 3 h, reflux;
85%
2-methyl-3-nitrochromen-4-one
59507-95-8

2-methyl-3-nitrochromen-4-one

(2-methoxyphenyl)-2,4-dimethyl-5-nitropyridine
100008-93-3

(2-methoxyphenyl)-2,4-dimethyl-5-nitropyridine

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: 83 percent / NaOEt / ethanol / 1.) 5 min, RT; 2.) 10 min, reflux
2: 85 percent / KOH / methanol / 1.) 1 h, reflux; 2.) 3 h, reflux
With potassium hydroxide; sodium ethanolate; In methanol; ethanol;

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