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Cas Database

100009-74-3

100009-74-3

Identification

  • Product Name:N-(2',3',4'-trimethoxyphenethyl)-2-bromo-4-methoxybenzamide

  • CAS Number: 100009-74-3

  • EINECS:

  • Molecular Weight:424.291

  • Molecular Formula: C19H22BrNO5

  • HS Code:

  • Mol File:100009-74-3.mol

Synonyms:N-(2',3',4'-trimethoxyphenethyl)-2-bromo-4-methoxybenzamide

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Relevant articles and documentsAll total 1 Articles be found

The structure of 2,3-dihydromenisporphine and the synthesis of dauriporphine, oxoisoaporphine alkaloids from Menispermum dauricum DC

Kunitomo,Kaede,Satoh

, p. 2778 - 2782 (2007/10/02)

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Process route upstream and downstream products

Process route

2-(2,3,4-trimethoxyphenyl)ethylamine
3937-16-4

2-(2,3,4-trimethoxyphenyl)ethylamine

2-Brom-4-methoxybenzoesaurechlorid
88741-40-6

2-Brom-4-methoxybenzoesaurechlorid

N-(2',3',4'-trimethoxyphenethyl)-2-bromo-4-methoxybenzamide
100009-74-3

N-(2',3',4'-trimethoxyphenethyl)-2-bromo-4-methoxybenzamide

Conditions
Conditions Yield
With sodium hydroxide; In diethyl ether; at 0 ℃; for 1h;
86.9%
2-bromo-4-methoxybenzoic acid
74317-85-4

2-bromo-4-methoxybenzoic acid

N-(2',3',4'-trimethoxyphenethyl)-2-bromo-4-methoxybenzamide
100009-74-3

N-(2',3',4'-trimethoxyphenethyl)-2-bromo-4-methoxybenzamide

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: SOCl2
2: 86.9 percent / 10 percent NaOH / diethyl ether / 1 h / 0 °C
With sodium hydroxide; thionyl chloride; In diethyl ether;
2-(2,3,4-trimethoxyphenyl)ethylamine
3937-16-4

2-(2,3,4-trimethoxyphenyl)ethylamine

2-Brom-4-methoxybenzoesaurechlorid
88741-40-6

2-Brom-4-methoxybenzoesaurechlorid

N-(2',3',4'-trimethoxyphenethyl)-2-bromo-4-methoxybenzamide
100009-74-3

N-(2',3',4'-trimethoxyphenethyl)-2-bromo-4-methoxybenzamide

Conditions
Conditions Yield
With sodium hydroxide; In diethyl ether; at 0 ℃; for 1h;
86.9%
2-bromo-4-methoxybenzoic acid
74317-85-4

2-bromo-4-methoxybenzoic acid

N-(2',3',4'-trimethoxyphenethyl)-2-bromo-4-methoxybenzamide
100009-74-3

N-(2',3',4'-trimethoxyphenethyl)-2-bromo-4-methoxybenzamide

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: SOCl2
2: 86.9 percent / 10 percent NaOH / diethyl ether / 1 h / 0 °C
With sodium hydroxide; thionyl chloride; In diethyl ether;

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