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Cas Database

1000300-07-1

1000300-07-1

Identification

  • Product Name:N-(5-cyano-7,8-dihydro-naphthalen-2-yl)-bezenesulfonamide

  • CAS Number: 1000300-07-1

  • EINECS:

  • Molecular Weight:310.376

  • Molecular Formula: C17H14N2O2S

  • HS Code:

  • Mol File:1000300-07-1.mol

Synonyms:N-(5-cyano-7,8-dihydro-naphthalen-2-yl)-bezenesulfonamide

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Relevant articles and documentsAll total 1 Articles be found

ARYLSULFONAMIDYL TETRALIN DERIVATIVES AND USES THEREOF

-

Page/Page column 53; 54, (2008/06/13)

Compounds of the formula I or pharmaceutically acceptable salts thereof, wherein Ar, X, m, R1, R2 are as defined herein. Also provided are methods for preparing, compositions comprising, and methods for using compounds of formula I for treatment of 5-HT6-mediated diseases.

Process route upstream and downstream products

Process route

N-(5-oxo-5,6,7,8-tetrahydro-naphthalen-2-yl)-benzenesulfonamide
1000300-06-0

N-(5-oxo-5,6,7,8-tetrahydro-naphthalen-2-yl)-benzenesulfonamide

trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

N-(5-cyano-7,8-dihydro-naphthalen-2-yl)-bezenesulfonamide
1000300-07-1

N-(5-cyano-7,8-dihydro-naphthalen-2-yl)-bezenesulfonamide

Conditions
Conditions Yield
N-(5-oxo-5,6,7,8-tetrahydro-naphthalen-2-yl)-benzenesulfonamide; trimethylsilyl cyanide; With zinc(II) iodide; for 15h;
With toluene-4-sulfonic acid; In toluene; for 3h; Heating / reflux;
44%
6-amino-1-tetralone
3470-53-9

6-amino-1-tetralone

N-(5-cyano-7,8-dihydro-naphthalen-2-yl)-bezenesulfonamide
1000300-07-1

N-(5-cyano-7,8-dihydro-naphthalen-2-yl)-bezenesulfonamide

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1.1: pyridine / 24 h / 23 °C
2.1: zinc(II) iodide / 15 h
2.2: 3 h / Heating / reflux
With pyridine; zinc(II) iodide;
benzenesulfonyl chloride
98-09-9

benzenesulfonyl chloride

N-(5-cyano-7,8-dihydro-naphthalen-2-yl)-bezenesulfonamide
1000300-07-1

N-(5-cyano-7,8-dihydro-naphthalen-2-yl)-bezenesulfonamide

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1.1: pyridine / 24 h / 23 °C
2.1: zinc(II) iodide / 15 h
2.2: 3 h / Heating / reflux
With pyridine; zinc(II) iodide;
N-(5-oxo-5,6,7,8-tetrahydro-naphthalen-2-yl)-benzenesulfonamide
1000300-06-0

N-(5-oxo-5,6,7,8-tetrahydro-naphthalen-2-yl)-benzenesulfonamide

trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

N-(5-cyano-7,8-dihydro-naphthalen-2-yl)-bezenesulfonamide
1000300-07-1

N-(5-cyano-7,8-dihydro-naphthalen-2-yl)-bezenesulfonamide

Conditions
Conditions Yield
N-(5-oxo-5,6,7,8-tetrahydro-naphthalen-2-yl)-benzenesulfonamide; trimethylsilyl cyanide; With zinc(II) iodide; for 15h;
With toluene-4-sulfonic acid; In toluene; for 3h; Heating / reflux;
44%
6-amino-1-tetralone
3470-53-9

6-amino-1-tetralone

N-(5-cyano-7,8-dihydro-naphthalen-2-yl)-bezenesulfonamide
1000300-07-1

N-(5-cyano-7,8-dihydro-naphthalen-2-yl)-bezenesulfonamide

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1.1: pyridine / 24 h / 23 °C
2.1: zinc(II) iodide / 15 h
2.2: 3 h / Heating / reflux
With pyridine; zinc(II) iodide;
benzenesulfonyl chloride
98-09-9

benzenesulfonyl chloride

N-(5-cyano-7,8-dihydro-naphthalen-2-yl)-bezenesulfonamide
1000300-07-1

N-(5-cyano-7,8-dihydro-naphthalen-2-yl)-bezenesulfonamide

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1.1: pyridine / 24 h / 23 °C
2.1: zinc(II) iodide / 15 h
2.2: 3 h / Heating / reflux
With pyridine; zinc(II) iodide;

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