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Cas Database

100032-60-8

100032-60-8

Identification

  • Product Name:N-[5-Methyl-thiazolidin-(2Z)-ylidene]-3-nitro-benzenesulfonamide

  • CAS Number: 100032-60-8

  • EINECS:

  • Molecular Weight:301.347

  • Molecular Formula:C10H11N3O4S2

  • HS Code:

  • Mol File:100032-60-8.mol

Synonyms:N-[5-Methyl-thiazolidin-(2Z)-ylidene]-3-nitro-benzenesulfonamide

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    Relevant articles and documentsAll total 1 Articles be found

    Consecutive Products of Sulphonamides. VI. Synthesis and Cyclization of N-Allyl-N'-arylsulphonyl-thioureas

    Hans, M.,Dehne, H.

    , p. 235 - 240 (2007/10/02)

    N-Allyl-N'-arylsulphonyl-thioureas 3a-e are synthesized by addition reaction of substituted arensulphonamides 2a-e and allylisothiocyanate 1.The thioureas 3a-e react with hydrogen bromide in acetic acid or bromine in chloroform to 2-(arylsulphonylimino)-5

    Process route upstream and downstream products

    Process route

    <i>N</i>-allyl-<i>N'</i>-(3-nitro-benzenesulfonyl)-thiourea
    100032-55-1

    N-allyl-N'-(3-nitro-benzenesulfonyl)-thiourea

    N-[5-Methyl-thiazolidin-(2Z)-ylidene]-3-nitro-benzenesulfonamide
    100032-60-8

    N-[5-Methyl-thiazolidin-(2Z)-ylidene]-3-nitro-benzenesulfonamide

    Conditions
    ConditionsYield
    With hydrogen bromide;Inacetic acid;for 1.16667h; Heating;
    93%
    3-nitrophenylsulfonamide
    121-52-8

    3-nitrophenylsulfonamide

    N-[5-Methyl-thiazolidin-(2Z)-ylidene]-3-nitro-benzenesulfonamide
    100032-60-8

    N-[5-Methyl-thiazolidin-(2Z)-ylidene]-3-nitro-benzenesulfonamide

    Conditions
    ConditionsYield
    Multi-step reaction with 2 steps
    1: 1.) NaOH / 1.) H2O, acetone; 2.) 5 h, reflux
    2: 93 percent / HBr / acetic acid / 1.17 h / Heating
    With sodium hydroxide; hydrogen bromide;Inacetic acid;
    <i>N</i>-allyl-<i>N'</i>-(3-nitro-benzenesulfonyl)-thiourea
    100032-55-1

    N-allyl-N'-(3-nitro-benzenesulfonyl)-thiourea

    N-[5-Methyl-thiazolidin-(2Z)-ylidene]-3-nitro-benzenesulfonamide
    100032-60-8

    N-[5-Methyl-thiazolidin-(2Z)-ylidene]-3-nitro-benzenesulfonamide

    Conditions
    ConditionsYield
    With hydrogen bromide;Inacetic acid;for 1.16667h; Heating;
    93%
    3-nitrophenylsulfonamide
    121-52-8

    3-nitrophenylsulfonamide

    N-[5-Methyl-thiazolidin-(2Z)-ylidene]-3-nitro-benzenesulfonamide
    100032-60-8

    N-[5-Methyl-thiazolidin-(2Z)-ylidene]-3-nitro-benzenesulfonamide

    Conditions
    ConditionsYield
    Multi-step reaction with 2 steps
    1: 1.) NaOH / 1.) H2O, acetone; 2.) 5 h, reflux
    2: 93 percent / HBr / acetic acid / 1.17 h / Heating
    With sodium hydroxide; hydrogen bromide;Inacetic acid;

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