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Cas Database

100032-61-9

100032-61-9

Identification

  • Product Name:N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-benzenesulfonamide

  • CAS Number: 100032-61-9

  • EINECS:

  • Molecular Weight:335.246

  • Molecular Formula: C10H11BrN2O2S2

  • HS Code:

  • Mol File:100032-61-9.mol

Synonyms:

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Relevant articles and documentsAll total 1 Articles be found

Consecutive Products of Sulphonamides. VI. Synthesis and Cyclization of N-Allyl-N'-arylsulphonyl-thioureas

Hans, M.,Dehne, H.

, p. 235 - 240 (2007/10/02)

N-Allyl-N'-arylsulphonyl-thioureas 3a-e are synthesized by addition reaction of substituted arensulphonamides 2a-e and allylisothiocyanate 1.The thioureas 3a-e react with hydrogen bromide in acetic acid or bromine in chloroform to 2-(arylsulphonylimino)-5

Process route upstream and downstream products

Process route

1-Allyl-3-phenylsulfonyl-thioharnstoff
74051-53-9

1-Allyl-3-phenylsulfonyl-thioharnstoff

N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-benzenesulfonamide
100032-61-9

N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-benzenesulfonamide

Conditions
Conditions Yield
With bromine; In chloroform; for 3h; Ambient temperature;
42%
benzenesulfonamide
98-10-2

benzenesulfonamide

N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-benzenesulfonamide
100032-61-9

N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-benzenesulfonamide

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: 1.) NaOH / 1.) H2O, acetone; 2.) 5 h, reflux
2: 42 percent / Br2 / CHCl3 / 3 h / Ambient temperature
With sodium hydroxide; bromine; In chloroform;
1-Allyl-3-phenylsulfonyl-thioharnstoff
74051-53-9

1-Allyl-3-phenylsulfonyl-thioharnstoff

N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-benzenesulfonamide
100032-61-9

N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-benzenesulfonamide

Conditions
Conditions Yield
With bromine; In chloroform; for 3h; Ambient temperature;
42%
benzenesulfonamide
98-10-2

benzenesulfonamide

N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-benzenesulfonamide
100032-61-9

N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-benzenesulfonamide

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: 1.) NaOH / 1.) H2O, acetone; 2.) 5 h, reflux
2: 42 percent / Br2 / CHCl3 / 3 h / Ambient temperature
With sodium hydroxide; bromine; In chloroform;

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