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Cas Database

100032-63-1

100032-63-1

Identification

  • Product Name:N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-4-chloro-benzenesulfonamide

  • CAS Number: 100032-63-1

  • EINECS:

  • Molecular Weight:369.691

  • Molecular Formula:C10H10BrClN2O2S2

  • HS Code:

  • Mol File:100032-63-1.mol

Synonyms:

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    Relevant articles and documentsAll total 1 Articles be found

    Consecutive Products of Sulphonamides. VI. Synthesis and Cyclization of N-Allyl-N'-arylsulphonyl-thioureas

    Hans, M.,Dehne, H.

    , p. 235 - 240 (2007/10/02)

    N-Allyl-N'-arylsulphonyl-thioureas 3a-e are synthesized by addition reaction of substituted arensulphonamides 2a-e and allylisothiocyanate 1.The thioureas 3a-e react with hydrogen bromide in acetic acid or bromine in chloroform to 2-(arylsulphonylimino)-5

    Process route upstream and downstream products

    Process route

    1-Allyl-3-(4-chlor-phenylsulfonyl)thioharnstoff
    90794-67-5

    1-Allyl-3-(4-chlor-phenylsulfonyl)thioharnstoff

    N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-4-chloro-benzenesulfonamide
    100032-63-1

    N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-4-chloro-benzenesulfonamide

    Conditions
    ConditionsYield
    With bromine;Inchloroform;for 3h; Ambient temperature;
    61%
    4-Chlorobenzenesulfonamide
    98-64-6

    4-Chlorobenzenesulfonamide

    N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-4-chloro-benzenesulfonamide
    100032-63-1

    N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-4-chloro-benzenesulfonamide

    Conditions
    ConditionsYield
    Multi-step reaction with 2 steps
    1: 1.) NaOH / 1.) H2O, acetone; 2.) 5 h, reflux
    2: 61 percent / Br2 / CHCl3 / 3 h / Ambient temperature
    With sodium hydroxide; bromine;Inchloroform;
    1-Allyl-3-(4-chlor-phenylsulfonyl)thioharnstoff
    90794-67-5

    1-Allyl-3-(4-chlor-phenylsulfonyl)thioharnstoff

    N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-4-chloro-benzenesulfonamide
    100032-63-1

    N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-4-chloro-benzenesulfonamide

    Conditions
    ConditionsYield
    With bromine;Inchloroform;for 3h; Ambient temperature;
    61%
    4-Chlorobenzenesulfonamide
    98-64-6

    4-Chlorobenzenesulfonamide

    N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-4-chloro-benzenesulfonamide
    100032-63-1

    N-[5-Bromomethyl-thiazolidin-(2Z)-ylidene]-4-chloro-benzenesulfonamide

    Conditions
    ConditionsYield
    Multi-step reaction with 2 steps
    1: 1.) NaOH / 1.) H2O, acetone; 2.) 5 h, reflux
    2: 61 percent / Br2 / CHCl3 / 3 h / Ambient temperature
    With sodium hydroxide; bromine;Inchloroform;

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