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Cas Database

100033-21-4

100033-21-4

Identification

  • Product Name:C16H10N9O4(1-)*Na(1+)

  • CAS Number: 100033-21-4

  • EINECS:

  • Molecular Weight:415.303

  • Molecular Formula: C16H10N9O4*Na

  • HS Code:

  • Mol File:100033-21-4.mol

Synonyms:

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Relevant articles and documentsAll total 1 Articles be found

Synthesis of 2,4-Bisalkyl(aryl)amino-6-cyanamino-s-triazines

Freiberg, Renate,Bulka, Ehrenfried

, p. 471 - 478 (2007/10/02)

Reaction of 2,4-bisalkyl(aryl)amino-6-chloro-s-triazines with disodiumcyanamide to 2,4-bisalkyl(aryl)amino-6-cyanamino-s-triazines (3a-g) strongly depends on the solvent used.In dimethylformamide by-products predominate.The best results are found in dimet

Process route upstream and downstream products

Process route

disodium cyanamide
20611-81-8

disodium cyanamide

6-chloro-N<SUP>2</SUP>,N<SUP>4</SUP>-bis(4-nitrophenyl)-1,3,5-triazine-2,4-diamine
2352-37-6

6-chloro-N2,N4-bis(4-nitrophenyl)-1,3,5-triazine-2,4-diamine

C<sub>16</sub>H<sub>10</sub>N<sub>9</sub>O<sub>4</sub><sup>(1-)</sup>*Na<sup>(1+)</sup>
100033-21-4

C16H10N9O4(1-)*Na(1+)

Conditions
Conditions Yield
In water; dimethyl sulfoxide; at 140 ℃; for 30h;
82%
6-chloro-N<SUP>2</SUP>,N<SUP>4</SUP>-bis(4-nitrophenyl)-1,3,5-triazine-2,4-diamine
2352-37-6

6-chloro-N2,N4-bis(4-nitrophenyl)-1,3,5-triazine-2,4-diamine

Sodium; 4,6-bis-(4-nitro-phenylamino)-[1,3,5]triazin-2-olate
100033-25-8

Sodium; 4,6-bis-(4-nitro-phenylamino)-[1,3,5]triazin-2-olate

C<sub>16</sub>H<sub>10</sub>N<sub>9</sub>O<sub>4</sub><sup>(1-)</sup>*Na<sup>(1+)</sup>
100033-21-4

C16H10N9O4(1-)*Na(1+)

Conditions
Conditions Yield
With water; disodium cyanamide; In N,N-dimethyl-formamide; at 130 - 140 ℃; for 0.5h;
19%
disodium cyanamide
20611-81-8

disodium cyanamide

6-chloro-N<SUP>2</SUP>,N<SUP>4</SUP>-bis(4-nitrophenyl)-1,3,5-triazine-2,4-diamine
2352-37-6

6-chloro-N2,N4-bis(4-nitrophenyl)-1,3,5-triazine-2,4-diamine

Sodium; 4,6-bis-(4-nitro-phenylamino)-[1,3,5]triazin-2-olate
100033-25-8

Sodium; 4,6-bis-(4-nitro-phenylamino)-[1,3,5]triazin-2-olate

C<sub>16</sub>H<sub>10</sub>N<sub>9</sub>O<sub>4</sub><sup>(1-)</sup>*Na<sup>(1+)</sup>
100033-21-4

C16H10N9O4(1-)*Na(1+)

Conditions
Conditions Yield
In water; N,N-dimethyl-formamide; at 130 - 140 ℃; for 0.5h;
19%
disodium cyanamide
20611-81-8

disodium cyanamide

6-chloro-N<SUP>2</SUP>,N<SUP>4</SUP>-bis(4-nitrophenyl)-1,3,5-triazine-2,4-diamine
2352-37-6

6-chloro-N2,N4-bis(4-nitrophenyl)-1,3,5-triazine-2,4-diamine

C<sub>16</sub>H<sub>10</sub>N<sub>9</sub>O<sub>4</sub><sup>(1-)</sup>*Na<sup>(1+)</sup>
100033-21-4

C16H10N9O4(1-)*Na(1+)

Conditions
Conditions Yield
In water; dimethyl sulfoxide; at 140 ℃; for 30h;
82%
6-chloro-N<SUP>2</SUP>,N<SUP>4</SUP>-bis(4-nitrophenyl)-1,3,5-triazine-2,4-diamine
2352-37-6

6-chloro-N2,N4-bis(4-nitrophenyl)-1,3,5-triazine-2,4-diamine

Sodium; 4,6-bis-(4-nitro-phenylamino)-[1,3,5]triazin-2-olate
100033-25-8

Sodium; 4,6-bis-(4-nitro-phenylamino)-[1,3,5]triazin-2-olate

C<sub>16</sub>H<sub>10</sub>N<sub>9</sub>O<sub>4</sub><sup>(1-)</sup>*Na<sup>(1+)</sup>
100033-21-4

C16H10N9O4(1-)*Na(1+)

Conditions
Conditions Yield
With water; disodium cyanamide; In N,N-dimethyl-formamide; at 130 - 140 ℃; for 0.5h;
19%
disodium cyanamide
20611-81-8

disodium cyanamide

6-chloro-N<SUP>2</SUP>,N<SUP>4</SUP>-bis(4-nitrophenyl)-1,3,5-triazine-2,4-diamine
2352-37-6

6-chloro-N2,N4-bis(4-nitrophenyl)-1,3,5-triazine-2,4-diamine

Sodium; 4,6-bis-(4-nitro-phenylamino)-[1,3,5]triazin-2-olate
100033-25-8

Sodium; 4,6-bis-(4-nitro-phenylamino)-[1,3,5]triazin-2-olate

C<sub>16</sub>H<sub>10</sub>N<sub>9</sub>O<sub>4</sub><sup>(1-)</sup>*Na<sup>(1+)</sup>
100033-21-4

C16H10N9O4(1-)*Na(1+)

Conditions
Conditions Yield
In water; N,N-dimethyl-formamide; at 130 - 140 ℃; for 0.5h;
19%

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