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Cas Database

1044579-39-6

1044579-39-6

Identification

  • Product Name:4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole

  • CAS Number: 1044579-39-6

  • EINECS:

  • Molecular Weight:370.414

  • Molecular Formula: C21H18N6O

  • HS Code:

  • Mol File:1044579-39-6.mol

Synonyms:4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole

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Relevant articles and documentsAll total 1 Articles be found

Convenient preparations of azo-dye labeled amino acids and amines

Katritzky, Alan Roy,Chen, Qi-Yin,Tala, Srinivasa Rao

supporting information; experimental part, p. 2400 - 2404 (2009/02/02)

N-(4-Arylazobenzoyl)-1H-benzotriazoles 3 react with amino acids 4 and amines 6 to give azo-dye labeled amino acids (5a-m) and amines (7a-n) in high yields (74-100%) with retention of chirality.

Process route upstream and downstream products

Process route

1-(methanesulfonyl)-1H-1,2,3-benzotriazole
37073-15-7

1-(methanesulfonyl)-1H-1,2,3-benzotriazole

p-methyl red
201858-51-7

p-methyl red

4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole
1044579-39-6

4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole

Conditions
Conditions Yield
With triethylamine; In tetrahydrofuran; for 5h; Reflux;
81%
4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole
1044579-39-6

4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole

4-[4-(dimethylamino)phenylazo]benzoyl-L-serine
1044579-48-7

4-[4-(dimethylamino)phenylazo]benzoyl-L-serine

Conditions
Conditions Yield
With triethylamine; In water; N,N-dimethyl-formamide; at 20 ℃; for 24h;
88%
4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole
1044579-39-6

4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole

4-[4-(dimethylamino)phenylazo]benzoyl-L-isoleucine
1044579-45-4

4-[4-(dimethylamino)phenylazo]benzoyl-L-isoleucine

Conditions
Conditions Yield
With triethylamine; In water; N,N-dimethyl-formamide; at 20 ℃; for 24h;
87%
4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole
1044579-39-6

4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole

phenylglycin
2835-06-5

phenylglycin

4-[(4-dimethylamino)phenylazo]benzoyl-DL-phenylglycine
113861-04-4

4-[(4-dimethylamino)phenylazo]benzoyl-DL-phenylglycine

Conditions
Conditions Yield
With triethylamine; In water; N,N-dimethyl-formamide; at 20 ℃; for 24h;
88%
4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole
1044579-39-6

4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole

4-[(4-dimethylamino)phenylazo]benzoylglycine
4238-39-5

4-[(4-dimethylamino)phenylazo]benzoylglycine

Conditions
Conditions Yield
With triethylamine; In water; N,N-dimethyl-formamide; at 20 ℃; for 24h;
99%
4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole
1044579-39-6

4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole

4-[4-(dimethylamino)phenylazo]benzoyl-L-typtophan
1044579-44-3

4-[4-(dimethylamino)phenylazo]benzoyl-L-typtophan

Conditions
Conditions Yield
With triethylamine; In water; N,N-dimethyl-formamide; at 20 ℃; for 24h;
90%
4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole
1044579-39-6

4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole

6-aminohexanoic acid
60-32-2,93208-38-9

6-aminohexanoic acid

4-[4-(dimethylamino)phenylazo]benzoyl-6-aminocaproic acid
885133-69-7

4-[4-(dimethylamino)phenylazo]benzoyl-6-aminocaproic acid

Conditions
Conditions Yield
With triethylamine; In water; N,N-dimethyl-formamide; at 20 ℃; for 24h;
95%
2-aminopyridine
504-29-0

2-aminopyridine

4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole
1044579-39-6

4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole

4-[4-(dimethylamino)phenylazo]benzoyl-2-aminopyridine
1044579-57-8

4-[4-(dimethylamino)phenylazo]benzoyl-2-aminopyridine

Conditions
Conditions Yield
With triethylamine; In N,N-dimethyl-formamide; at 150 ℃;
84%
4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole
1044579-39-6

4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole

4-[4-(dimethylamino)phenylazo]benzoyl-L-alanine
1044579-42-1

4-[4-(dimethylamino)phenylazo]benzoyl-L-alanine

Conditions
Conditions Yield
With triethylamine; In water; N,N-dimethyl-formamide; at 20 ℃; for 24h;
81%
4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole
1044579-39-6

4-[(4-dimethylamino)phenylazo]benzoyl-1H-benzotriazole

4-[4-(dimethylamino)phenylazo]benzoyl-L-methionine
1044579-46-5

4-[4-(dimethylamino)phenylazo]benzoyl-L-methionine

Conditions
Conditions Yield
With triethylamine; In water; N,N-dimethyl-formamide; at 20 ℃; for 24h;
81%

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