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Cas Database

1072006-74-6

1072006-74-6

Identification

  • Product Name:2-phenyl-2-piperidin-1-yl-cyclopropanecarboxylic acid n-butyl ester

  • CAS Number: 1072006-74-6

  • EINECS:

  • Molecular Weight:301.429

  • Molecular Formula: C19H27NO2

  • HS Code:

  • Mol File:1072006-74-6.mol

Synonyms:

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Relevant articles and documentsAll total 1 Articles be found

Copper(0)-induced aminocyclopropanation of olefins via deselenation of N,N-disubstituted aromatic selenoamides

Mitamura, Takenori,Nomoto, Akihiro,Sonoda, Motohiro,Ogawa, Akiya

experimental part, p. 9983 - 9988 (2009/04/03)

Upon heating of a mixture of N,N-disubstituted aromatic selenoamides and several electron-deficient olefins in the presence of copper(0) powder, a novel deselenative cyclopropanation takes place to afford the corresponding aminocyclopropanes in good yields. When acrylonitrile is employed as an electron-deficient olefin, the aminocyclopentanation occurs in preference to the aminocyclopropanation by prolonging the reaction time. The obtained aminocyclopropane derivatives can be converted to the corresponding 1,4-dicarbonyl compounds upon treatment with 2 N HCl.

Process route upstream and downstream products

Process route

acrylic acid n-butyl ester
141-32-2,9003-49-0

acrylic acid n-butyl ester

N-(phenylselenocarbonyl) piperidine
100033-95-2

N-(phenylselenocarbonyl) piperidine

2-phenyl-2-piperidin-1-yl-cyclopropanecarboxylic acid n-butyl ester
1072006-74-6

2-phenyl-2-piperidin-1-yl-cyclopropanecarboxylic acid n-butyl ester

C<sub>26</sub>H<sub>32</sub>
854247-68-0

C26H32

Conditions
Conditions Yield
With copper; at 110 ℃; for 4h;
66%
15%
acrylic acid n-butyl ester
141-32-2,9003-49-0

acrylic acid n-butyl ester

N-(phenylselenocarbonyl) piperidine
100033-95-2

N-(phenylselenocarbonyl) piperidine

2-phenyl-2-piperidin-1-yl-cyclopropanecarboxylic acid n-butyl ester
1072006-74-6

2-phenyl-2-piperidin-1-yl-cyclopropanecarboxylic acid n-butyl ester

C<sub>26</sub>H<sub>32</sub>
854247-68-0

C26H32

Conditions
Conditions Yield
With copper; at 110 ℃; for 4h;
66%
15%

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