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Cas Database

1082488-99-0

1082488-99-0

Identification

  • Product Name:4-(4-dimethylaminophenylazo)benzoyl fluoride

  • CAS Number: 1082488-99-0

  • EINECS:

  • Molecular Weight:271.294

  • Molecular Formula: C15H14FN3O

  • HS Code:

  • Mol File:1082488-99-0.mol

Synonyms:

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Relevant articles and documentsAll total 1 Articles be found

Use of C,N-chelated di-n-butyltin(IV) fluoride for the synthesis of acyl fluorides, fluoroformates and fluorophosgene

?vec, Petr,Eisner, Ale?,Kolá?ová, Lenka,Weidlich, Tomá?,Pejchal, Vladimír,R??i?ka, Ale?

, p. 6320 - 6323 (2008)

{2-[(CH3)2NCH2]C6H4}(n-Bu)2SnF (1) reacts with various chloroformates, acyl chlorides, methanesulfonyl chloride, 4,4′-dimethoxytrityl chloride and phosgene precursors or derivatives to form fluorinated analogues. All reactions proceed rapidly and under mild conditions. The use of a catalytic amount of 1 and KF in toluene led to a relatively high yield of a selected fluoroformate.

Process route upstream and downstream products

Process route

N,N-dimethyl-p-aminophenylazobenzoyl chloride
27128-58-1

N,N-dimethyl-p-aminophenylazobenzoyl chloride

4-(4-dimethylaminophenylazo)benzoyl fluoride
1082488-99-0

4-(4-dimethylaminophenylazo)benzoyl fluoride

Conditions
Conditions Yield
With 2-[(CH3)2NCH2](C6H4)(n-Bu)2SnF; In benzene; at 20 ℃; for 1h; Inert atmosphere;
82 %Spectr.

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