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Cas Database

112-84-5

112-84-5

Identification

  • Product Name:Erucylamide

  • CAS Number: 112-84-5

  • EINECS:204-009-2

  • Molecular Weight:337.59

  • Molecular Formula: C22H43NO

  • HS Code:29241990

  • Mol File:112-84-5.mol

Synonyms:13-Docosenamide, (13Z)-;13-Docosenamide,(Z)- (8CI);Erucamide (6CI);Adogen 58;Alflow 10;Alflow P 10;Amide E;Ampacet 10090;Armid E;Armoslip E;Armoslip EPX;Armoslip EXP;Atmer 1753;Atmer SA 1753;Atmer SA 1753FD;Chemstat HTSA 22;Chemstat HTSA 22-20M;Crodamide E;Crodamide ER;Diamid L 200;E 10 (amide);Erucic acid amide;Erucic amide;Erucoyl amide;Erucyl amide;Fatty Amide E;Kemamide E;KemamideE Ultra;Loxamid E;Lutamide ER;Neutron S;cis-13-Docosenamide;Erucylamide(Erucic acid amide);Docosenoic Acidamide;

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Safety information and MSDS view more

  • Pictogram(s):IrritantXi

  • Hazard Codes:Xi

  • Signal Word:No signal word.

  • Hazard Statement:none

  • First-aid measures: General adviceConsult a physician. Show this safety data sheet to the doctor in attendance.If inhaled If breathed in, move person into fresh air. If not breathing, give artificial respiration. Consult a physician. In case of skin contact Wash off with soap and plenty of water. Consult a physician. In case of eye contact Rinse thoroughly with plenty of water for at least 15 minutes and consult a physician. If swallowed Never give anything by mouth to an unconscious person. Rinse mouth with water. Consult a physician.

  • Fire-fighting measures: Suitable extinguishing media Use water spray, alcohol-resistant foam, dry chemical or carbon dioxide. Wear self-contained breathing apparatus for firefighting if necessary.

  • Accidental release measures: Use personal protective equipment. Avoid dust formation. Avoid breathing vapours, mist or gas. Ensure adequate ventilation. Evacuate personnel to safe areas. Avoid breathing dust. For personal protection see section 8. Prevent further leakage or spillage if safe to do so. Do not let product enter drains. Discharge into the environment must be avoided. Pick up and arrange disposal. Sweep up and shovel. Keep in suitable, closed containers for disposal.

  • Handling and storage: Avoid contact with skin and eyes. Avoid formation of dust and aerosols. Avoid exposure - obtain special instructions before use.Provide appropriate exhaust ventilation at places where dust is formed. For precautions see section 2.2. Store in cool place. Keep container tightly closed in a dry and well-ventilated place.

  • Exposure controls/personal protection:Occupational Exposure limit valuesBiological limit values Handle in accordance with good industrial hygiene and safety practice. Wash hands before breaks and at the end of workday. Eye/face protection Safety glasses with side-shields conforming to EN166. Use equipment for eye protection tested and approved under appropriate government standards such as NIOSH (US) or EN 166(EU). Skin protection Wear impervious clothing. The type of protective equipment must be selected according to the concentration and amount of the dangerous substance at the specific workplace. Handle with gloves. Gloves must be inspected prior to use. Use proper glove removal technique(without touching glove's outer surface) to avoid skin contact with this product. Dispose of contaminated gloves after use in accordance with applicable laws and good laboratory practices. Wash and dry hands. The selected protective gloves have to satisfy the specifications of EU Directive 89/686/EEC and the standard EN 374 derived from it. Respiratory protection Wear dust mask when handling large quantities. Thermal hazards

Supplier and reference price

  • Manufacture/Brand
  • Product Description
  • Packaging
  • Price
  • Delivery
  • Purchase
  • Manufacture/Brand:TRC
  • Product Description:cis-13-Docosenamide
  • Packaging:10g
  • Price:$ 70
  • Delivery:In stock
  • Buy Now
  • Manufacture/Brand:TCI Chemical
  • Product Description:Erucamide >85.0%(GC)
  • Packaging:25g
  • Price:$ 38
  • Delivery:In stock
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  • Manufacture/Brand:TCI Chemical
  • Product Description:Erucamide >85.0%(GC)
  • Packaging:100g
  • Price:$ 70
  • Delivery:In stock
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  • Manufacture/Brand:TCI Chemical
  • Product Description:Erucamide >85.0%(GC)
  • Packaging:500g
  • Price:$ 148
  • Delivery:In stock
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  • Manufacture/Brand:Sigma-Aldrich
  • Product Description:Plastic additive 13 United States Pharmacopeia (USP) Reference Standard
  • Packaging:100mg
  • Price:$ 169
  • Delivery:In stock
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  • Manufacture/Brand:Sigma-Aldrich
  • Product Description:cis-13-Docosenoamide
  • Packaging:100g
  • Price:$ 76.3
  • Delivery:In stock
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  • Manufacture/Brand:Sigma-Aldrich
  • Product Description:cis-13-Docosenoamide
  • Packaging:5g
  • Price:$ 40.3
  • Delivery:In stock
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  • Manufacture/Brand:Frontier Specialty Chemicals
  • Product Description:Erucamide 98%
  • Packaging:25g
  • Price:$ 22
  • Delivery:In stock
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  • Manufacture/Brand:Frontier Specialty Chemicals
  • Product Description:Erucamide 98%
  • Packaging:100g
  • Price:$ 72
  • Delivery:In stock
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  • Manufacture/Brand:Crysdot
  • Product Description:(Z)-Docos-13-enamide 95+%
  • Packaging:500g
  • Price:$ 96
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Relevant articles and documentsAll total 2 Articles be found

Method and apparatus for manufacturing carboxylic acid amide compound

-

Paragraph 0059-0062; 0076, (2017/06/02)

The present invention relates to a process and an apparatus for producing a carboxylic acid amide compound, and more particularly, to a process for producing a carboxylic acid amide compound which alternately performs a reaction process of a first manufacturing process that promotes the reaction between a first carboxylic acid and a first ammonia in the presence of a first catalyst and a reaction process of a second manufacturing process that promotes the reaction between a second carboxylic acid and a first ammonia in the presence of a second catalyst wherein each of them is progressed alternately between each preparation process so that the reaction between the carboxylic acid and the ammonia, which is intermittently carried out by the respective preparation processes, can be continuously performed, and moreover, the time required for the respective preparation processes is shortened, so that the carboxylic acid amide compound can be produced in a large amount in a short time.

Electrospray ionization and collision induced dissociation mass spectrometry of primary fatty acid amides

Divito, Erin B.,Davic, Andrew P.,Johnson, Mitchell E.,Cascio, Michael

experimental part, p. 2388 - 2394 (2012/07/27)

Primary fatty acid amides are a group of bioactive lipids that have been linked with a variety of biological processes such as sleep regulation and modulation of monoaminergic systems. As novel forms of these molecules continue to be discovered, more emphasis will be placed on selective, trace detection. Currently, there is no published experimental determination of collision induced dissociation of PFAMs. A select group of PFAM standards, 12 to 22 length carbon chains, were directly infused into an electrospray ionization source Quadrupole Time of Flight Mass Spectrometer. All standards were monitored in positive mode using the [M + H]+ peak. Mass Hunter Qualitative Analysis software was used to calculate empirical formulas of the product ions. All PFAMs showed losses of 14 m/z indicative of an acyl chain, while the monounsaturated group displayed neutral losses corresponding to H2O and NH3. The resulting spectra were used to propose fragmentation mechanisms. Isotopically labeled PFAMs were used to validate the proposed mechanisms. Patterns of saturated versus unsaturated standards were distinctive, allowing for simple differentiation. This determination will allow for fast, qualitative identification of PFAMs. Additionally, it will provide a method development tool for selection of unique product ions when analyzed in multiple reaction monitoring mode.

Process route upstream and downstream products

Process route

cis-13-docosenoic acid
112-86-7

cis-13-docosenoic acid

Unislip 1753
112-84-5

Unislip 1753

Conditions
Conditions Yield
With ammonia; zircornium(IV) n-propoxide; at 165 ℃; for 6h; Reagent/catalyst;
98.8%
Multi-step reaction with 2 steps
1: oxalyl dichloride / dichloromethane / Inert atmosphere
2: ammonium hydroxide
With ammonium hydroxide; oxalyl dichloride; In dichloromethane;
erucic acid chloride
59044-32-5,7459-29-2

erucic acid chloride

Unislip 1753
112-84-5

Unislip 1753

Conditions
Conditions Yield
With ammonium hydroxide;
Unislip 1753
112-84-5

Unislip 1753

erucyl alcohol
629-98-1

erucyl alcohol

Conditions
Conditions Yield
With samarium diiodide; water; triethylamine; In tetrahydrofuran; at 23 ℃; for 18h; chemoselective reaction; Inert atmosphere;
94%
[hydroxy(tosyloxy)iodo]benzene
27126-76-7

[hydroxy(tosyloxy)iodo]benzene

Unislip 1753
112-84-5

Unislip 1753

cis-12-heneicosenylammonium tosylate
116749-38-3

cis-12-heneicosenylammonium tosylate

Conditions
Conditions Yield
In acetonitrile; at 65 - 70 ℃; for 0.0333333h;
63%
Unislip 1753
112-84-5

Unislip 1753

cis-docos-13-enylamine
26398-95-8

cis-docos-13-enylamine

Conditions
Conditions Yield
With lithium aluminium tetrahydride; In tetrahydrofuran; for 12h; Reflux;
100%
Unislip 1753
112-84-5

Unislip 1753

(3R)-N-{(3R,6R,9R,12S,15R,18S,19R)-6-(3-amino-3-oxopropyl)-15-[(2S)-butan-2-yl]-12-(4-hydroxybenzyl)-9-[(1R)-1-hydroxyethyl]-3,19-dimethyl-2,5,8,11,14,17-hexaoxo-1-oxa-4,7,10,13,16-pentaazacyclononadecan-18-yl}-15-carbamimidamido-3-hydroxypentadecanamide

(3R)-N-{(3R,6R,9R,12S,15R,18S,19R)-6-(3-amino-3-oxopropyl)-15-[(2S)-butan-2-yl]-12-(4-hydroxybenzyl)-9-[(1R)-1-hydroxyethyl]-3,19-dimethyl-2,5,8,11,14,17-hexaoxo-1-oxa-4,7,10,13,16-pentaazacyclononadecan-18-yl}-15-carbamimidamido-3-hydroxypentadecanamide

Conditions
Conditions Yield
Multi-step reaction with 9 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / Reflux
2.1: sodium hydrogencarbonate / 1,4-dioxane; water / 14 h / 0 - 20 °C
3.1: ozone / dichloromethane / 0.5 h / -78 °C / Inert atmosphere
3.2: 0.5 h / -78 - 10 °C / Inert atmosphere
4.1: (R,R)-(η5-cyclopentadienyl)chloro[(4R,trans)-2,2-dimethyl-α,α,α',α'-tetraphenyl-1,3-dioxolane-4,5-dimethanolato]titanium / tetrahydrofuran; diethyl ether / 4 h / 0 - 20 °C
4.2: 16 h / -78 - 20 °C
5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 13 h / 0 - 20 °C
5.2: 12 h / 20 °C
5.3: 120 h / Inert atmosphere
6.1: ozone / dichloromethane / 0.5 h / -78 °C / Inert atmosphere
6.2: 12 h / -78 - 20 °C / Inert atmosphere
7.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 2 h / 20 °C
8.1: 4-methyl-morpholine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h
8.2: 70 h / 20 °C
9.1: trifluoroacetic acid / dichloromethane; water / 1 h / 20 °C
With 4-methyl-morpholine; sodium chlorite; sodium dihydrogenphosphate; lithium aluminium tetrahydride; 2-methyl-but-2-ene; (R,R)-(η5-cyclopentadienyl)chloro[(4R,trans)-2,2-dimethyl-α,α,α',α'-tetraphenyl-1,3-dioxolane-4,5-dimethanolato]titanium; sodium hydrogencarbonate; ozone; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
Unislip 1753
112-84-5

Unislip 1753

di-tert-butyl [(E){[(13R)-15-({(3R,6R,9R,12S,15R,18S,19R)-6-(3-amino-3-oxopropyl)-15-[(2S)-butan-2-yl]-12-(4-hydroxybenzyl)-9-[(1R)-1-hydroxyethyl]-3,19-dimethyl-2,5,8,11,14,17-hexaoxo-1-oxa-4,7,10,13,16-pentaazacyclononadecan-18-yl}amino)-13-(methoxymethoxy)-15-oxopentadecyl]amino}methylylidene]biscarbamate

di-tert-butyl [(E){[(13R)-15-({(3R,6R,9R,12S,15R,18S,19R)-6-(3-amino-3-oxopropyl)-15-[(2S)-butan-2-yl]-12-(4-hydroxybenzyl)-9-[(1R)-1-hydroxyethyl]-3,19-dimethyl-2,5,8,11,14,17-hexaoxo-1-oxa-4,7,10,13,16-pentaazacyclononadecan-18-yl}amino)-13-(methoxymethoxy)-15-oxopentadecyl]amino}methylylidene]biscarbamate

Conditions
Conditions Yield
Multi-step reaction with 8 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / Reflux
2.1: sodium hydrogencarbonate / 1,4-dioxane; water / 14 h / 0 - 20 °C
3.1: ozone / dichloromethane / 0.5 h / -78 °C / Inert atmosphere
3.2: 0.5 h / -78 - 10 °C / Inert atmosphere
4.1: (R,R)-(η5-cyclopentadienyl)chloro[(4R,trans)-2,2-dimethyl-α,α,α',α'-tetraphenyl-1,3-dioxolane-4,5-dimethanolato]titanium / tetrahydrofuran; diethyl ether / 4 h / 0 - 20 °C
4.2: 16 h / -78 - 20 °C
5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 13 h / 0 - 20 °C
5.2: 12 h / 20 °C
5.3: 120 h / Inert atmosphere
6.1: ozone / dichloromethane / 0.5 h / -78 °C / Inert atmosphere
6.2: 12 h / -78 - 20 °C / Inert atmosphere
7.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 2 h / 20 °C
8.1: 4-methyl-morpholine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h
8.2: 70 h / 20 °C
With 4-methyl-morpholine; sodium chlorite; sodium dihydrogenphosphate; lithium aluminium tetrahydride; 2-methyl-but-2-ene; (R,R)-(η5-cyclopentadienyl)chloro[(4R,trans)-2,2-dimethyl-α,α,α',α'-tetraphenyl-1,3-dioxolane-4,5-dimethanolato]titanium; sodium hydrogencarbonate; ozone; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;

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