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Cas Database

1256931-87-9

1256931-87-9

Identification

  • Product Name:([5-oxo-1,10-phenanthroline-6(5H)-ylidene]benzoylhydrazide)chlorotricarbonylrhenium(I)

  • CAS Number: 1256931-87-9

  • EINECS:

  • Molecular Weight:634.021

  • Molecular Formula: C22H12ClN4O5Re

  • HS Code:

  • Mol File:1256931-87-9.mol

Synonyms:

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Relevant articles and documentsAll total 1 Articles be found

Tricarbonyl rhenium(I) and technetium(I) complexes with hydrazones derived from 4,5-diazafluoren-9-one and 1,10-phenanthroline-5,6-dione

Barbazan, Paula,Hagenbach, Adelheid,Oehlke, Elisabeth,Abram, Ulrich,Carballo, Rosa,Rodriguez-Hermida, Sabina,Vazquez-Lopez, Ezequiel M.

, p. 4622 - 4630 (2010)

Tricarbonylrhenium(I) and -technetium(I) halide (halide = Cl and Br) complexes of ligands derived from 4,5-diazafluoren-9-one (df) and 1,10-phenanthroline-5,6-dione (phen) derivatives of benzoic and 2-hydroxybenzoic acid hydrazides have been prepared. The

Process route upstream and downstream products

Process route

fac-bis(acetonitrile)chlorotricarbonylrhenium(I)
28862-29-5,678142-40-0

fac-bis(acetonitrile)chlorotricarbonylrhenium(I)

[5-oxo-1,10-phenanthroline-6(5H)-ylidene]benzohydrazide

[5-oxo-1,10-phenanthroline-6(5H)-ylidene]benzohydrazide

([5-oxo-1,10-phenanthroline-6(5H)-ylidene]benzoylhydrazide)chlorotricarbonylrhenium(I)
1256931-87-9

([5-oxo-1,10-phenanthroline-6(5H)-ylidene]benzoylhydrazide)chlorotricarbonylrhenium(I)

Conditions
Conditions Yield
In chloroform; mixt. of Re complex and ligand (Re:L=1:1) in dry CHCl3 refluxed for 2.5 h; filtered, dried (vac., CaCl2), elem. anal.;
86.1%

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