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125867-97-2

125867-97-2

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Relevant articles and documentsAll total 1 Articles be found

Synthese oligomerer Biocide auf der Basis von Oxyethylenglycol-Traegern

Schnabelrauch, Matthias,Carlsohn, Hartmut,Heinze, Thomas,Hartmann, Manfred,Klemm, Dieter

, p. 280 - 281 (2007/10/02)

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Process route upstream and downstream products

Process route

diethylene glycol benzoate
20587-61-5

diethylene glycol benzoate

Succinic acid 3-{3-[2-(2-benzoyloxy-ethoxy)-ethoxycarbonyl]-propionyloxy}-2-bromo-2-nitro-propyl ester 2-(2-benzoyloxy-ethoxy)-ethyl ester
125867-97-2

Succinic acid 3-{3-[2-(2-benzoyloxy-ethoxy)-ethoxycarbonyl]-propionyloxy}-2-bromo-2-nitro-propyl ester 2-(2-benzoyloxy-ethoxy)-ethyl ester

Conditions
Conditions Yield
Multi-step reaction with 2 steps
2: 1) pyridine, Cl-COOEt / 1) ether, -10 degC, 20 min.; 2) ether, 24 h, room temp.
With pyridine; chloroformic acid ethyl ester;
benzoyl chloride
98-88-4

benzoyl chloride

Succinic acid 3-{3-[2-(2-benzoyloxy-ethoxy)-ethoxycarbonyl]-propionyloxy}-2-bromo-2-nitro-propyl ester 2-(2-benzoyloxy-ethoxy)-ethyl ester
125867-97-2

Succinic acid 3-{3-[2-(2-benzoyloxy-ethoxy)-ethoxycarbonyl]-propionyloxy}-2-bromo-2-nitro-propyl ester 2-(2-benzoyloxy-ethoxy)-ethyl ester

Conditions
Conditions Yield
Multi-step reaction with 3 steps
1: pyridine
3: 1) pyridine, Cl-COOEt / 1) ether, -10 degC, 20 min.; 2) ether, 24 h, room temp.
With pyridine; chloroformic acid ethyl ester;
2-bromo-2-nitro-1,3-propanediol
52-51-7

2-bromo-2-nitro-1,3-propanediol

Succinic acid mono-[2-(2-benzoyloxy-ethoxy)-ethyl] ester
125867-95-0

Succinic acid mono-[2-(2-benzoyloxy-ethoxy)-ethyl] ester

Succinic acid 2-(2-benzoyloxy-ethoxy)-ethyl ester 2-bromo-3-hydroxy-2-nitro-propyl ester
125867-96-1

Succinic acid 2-(2-benzoyloxy-ethoxy)-ethyl ester 2-bromo-3-hydroxy-2-nitro-propyl ester

Succinic acid 3-{3-[2-(2-benzoyloxy-ethoxy)-ethoxycarbonyl]-propionyloxy}-2-bromo-2-nitro-propyl ester 2-(2-benzoyloxy-ethoxy)-ethyl ester
125867-97-2

Succinic acid 3-{3-[2-(2-benzoyloxy-ethoxy)-ethoxycarbonyl]-propionyloxy}-2-bromo-2-nitro-propyl ester 2-(2-benzoyloxy-ethoxy)-ethyl ester

Conditions
Conditions Yield
With pyridine; chloroformic acid ethyl ester; Yield given. Multistep reaction. Yields of byproduct given; 1) ether, -10 degC, 20 min.; 2) ether, 24 h, room temp.;

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