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14952-08-0

14952-08-0

Identification

Synonyms:[R,(+)]-3-O-Benzyl-2-O-stearoyl-L-glycerol

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Relevant articles and documentsAll total 2 Articles be found

Synthesis of glyceryletherphosphatides, 1st communication. Preparation of 1-0-octadecyl-2-0-acetyl-sn-glyceryl-3-phosphorylcholine ('platelet activating factor'), of its enantiomer and of some analogous compounds

Hirth,Barner

, p. 1059 - 1084 (2007/10/02)

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Process route upstream and downstream products

Process route

benzyl chloride
100-44-7

benzyl chloride

β-Stearoyl-D-α-glycerylbenzylaether
14952-08-0

β-Stearoyl-D-α-glycerylbenzylaether

Conditions
Conditions Yield
Multi-step reaction with 3 steps
1: 94 percent / 30percent NaOH / tributylbenzylammonium chloride / 4 h / 50 °C
2: 91 percent / 1N H2SO4 / 1 h / 90 °C
3: pyridine / tetrahydrofuran / Ambient temperature
With pyridine; sodium hydroxide; sulfuric acid; benzyltri(n-butyl)ammonium chloride; In tetrahydrofuran;
(R)-3-benzyloxy-1,2-propanediol
56552-80-8

(R)-3-benzyloxy-1,2-propanediol

Stearoyl chloride
112-76-5

Stearoyl chloride

β-Stearoyl-D-α-glycerylbenzylaether
14952-08-0

β-Stearoyl-D-α-glycerylbenzylaether

3-O-Benzyl-1-O-octadecanoyl-sn-glycerin
4145-51-1,6236-22-2,116947-35-4,988-76-1

3-O-Benzyl-1-O-octadecanoyl-sn-glycerin

3-O-benzyl-1,2-dioctadecanoyl-sn-glycerol
56586-08-4,7145-33-7

3-O-benzyl-1,2-dioctadecanoyl-sn-glycerol

Conditions
Conditions Yield
With pyridine; In tetrahydrofuran; Ambient temperature;
38%
(S)-4-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxolane
16495-03-7

(S)-4-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxolane

β-Stearoyl-D-α-glycerylbenzylaether
14952-08-0

β-Stearoyl-D-α-glycerylbenzylaether

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: 91 percent / 1N H2SO4 / 1 h / 90 °C
2: pyridine / tetrahydrofuran / Ambient temperature
With pyridine; sulfuric acid; In tetrahydrofuran;
β-Stearoyl-D-α-glycerylbenzylaether
14952-08-0

β-Stearoyl-D-α-glycerylbenzylaether

Conditions
Conditions Yield
D-α-Trityl-β-stearoylglyceryl-α'-benzylaether (II), Detritylierung bei Chromatographie an SiO2;
entspr. Trityl-acyl-benzyl-glycerin, Chromatograph. an Kieselsaeure/Borsaeure;

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