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19117-31-8

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19117-31-8 Usage

Uses

Reactant for:Anti-SN2′ Mitsunobu reaction with chiral hydroxy-alpha-alkenylsilanes to give vinylsilanesAnodic oxidation reactions

Check Digit Verification of cas no

The CAS Registry Mumber 19117-31-8 includes 8 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 5 digits, 1,9,1,1 and 7 respectively; the second part has 2 digits, 3 and 1 respectively.
Calculate Digit Verification of CAS Registry Number 19117-31:
(7*1)+(6*9)+(5*1)+(4*1)+(3*7)+(2*3)+(1*1)=98
98 % 10 = 8
So 19117-31-8 is a valid CAS Registry Number.
InChI:InChI=1/C10H15NS/c1-10(2,3)11-12-9-7-5-4-6-8-9/h4-8,11H,1-3H3

19117-31-8 Well-known Company Product Price

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  • TCI America

  • (B2240)  N-tert-Butylbenzenesulfenamide  >96.0%(GC)

  • 19117-31-8

  • 1g

  • 490.00CNY

  • Detail
  • TCI America

  • (B2240)  N-tert-Butylbenzenesulfenamide  >96.0%(GC)

  • 19117-31-8

  • 5g

  • 1,290.00CNY

  • Detail
  • TCI America

  • (B2240)  N-tert-Butylbenzenesulfenamide  >96.0%(GC)

  • 19117-31-8

  • 25g

  • 4,490.00CNY

  • Detail
  • Aldrich

  • (681792)  N-tert-Butylbenzenesulfenamide  97%

  • 19117-31-8

  • 681792-1G

  • 540.54CNY

  • Detail
  • Aldrich

  • (681792)  N-tert-Butylbenzenesulfenamide  97%

  • 19117-31-8

  • 681792-5G

  • 2,241.72CNY

  • Detail

19117-31-8SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 11, 2017

Revision Date: Aug 11, 2017

1.Identification

1.1 GHS Product identifier

Product name 2-methyl-N-phenylsulfanylpropan-2-amine

1.2 Other means of identification

Product number -
Other names N-(1,1-Dimethylethyl)benzenesulfenamide

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:19117-31-8 SDS

19117-31-8Relevant articles and documents

Cardin et al.

, p. C59,C60 (1972)

Comparison of conventional and microwave-assisted synthesis of some new sulfenamides under free catalyst and ligand

Yakan, Hasan,Kütük, Halil

, p. 2047 - 2057 (2018/09/25)

Abstract: Sulfenamide and its derivatives (S–N bond) have been synthesized with classical method in the literature. However, microwave-assisted synthesis of a series of N-(substituted phenylthio), N-(benzylthio), N-(cyclothio), and N-(2-mercaptobenzimidazolyl)amines has been not in the literature yet. They have been obtained from treating some amines (4?mmol) with thiophthalimides (PhthSR, 1?mmol) using sulfur transfer reagent in the presence of 2-ethoxyethanol (β-ee, neat) under microwave irradiation at 50?°C. The scope of this reaction was shown by the efficient synthesis of sulfenamides in good to excellent yields of 70–98% under free catalyst and ligand. Nine of the synthesized sulfenamide derivatives are novel. All of the thiols react with morpholine to give corresponding sulfenamides in excellent yields of 78–98%. Thiophenol, 4-methylthiophenol, 4-chlorothiophenol, and 4-fluorothiophenol react with cyclohexylamine to give corresponding sulfenamides in high yields 81–92%. Thiophenol, 4-methylthiophenol, 4-chlorothiophenol react with pyrrolidine to give corresponding sulfenamides in good yields of 70–76%. We observed that the reaction of t-butylamine with N-(phenylthio)phthalimide gave desired sulfenamide under microwave irradiation in the presence of DPPH as radical scavenger reagent in high yield of 93%. Aniline, benzylamine, 1-hexylamine, ethanolamine, diethylamine, N-ethyl-n-butylamine, N-ethylaniline, N-benzylmethylamine, t-butylamine react with thiols to give symmetrical disulfides instead of desired products under microwave irradiation, 2-ethoxyethanol as a solvent (neat), and at 50?°C. In this study, microwave-assisted synthesis method was compared with the classical method. All the products obtained were purified with chromatographic method and the analysis of these products was confirmed with IR, 1H NMR, 13C NMR spectroscopy, MS spectrometry, and elemental methods. Graphical abstract: [Figure not available: see fulltext.].

Copper-catalyzed synthesis of sulfenamides utilizing diaryl disulfides with alkyl amines

Taniguchi, Nobukazu

, p. 1917 - 1920 (2008/03/13)

The copper-catalyzed coupling of diaryl disulfides with alkyl amines can afford various sulfenamides in good yields. Furthermore, the present reaction is efficient and can be used for both of the aryl sulfide groups on disulfide. Georg Thieme Verlag Stutt

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