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2224-15-9 Usage

Uses

Ethylene Glycol Diglycidyl Ether is commonly added to asorbants because of it high carbon dioxide absorbing capacity.

Check Digit Verification of cas no

The CAS Registry Mumber 2224-15-9 includes 7 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 4 digits, 2,2,2 and 4 respectively; the second part has 2 digits, 1 and 5 respectively.
Calculate Digit Verification of CAS Registry Number 2224-15:
(6*2)+(5*2)+(4*2)+(3*4)+(2*1)+(1*5)=49
49 % 10 = 9
So 2224-15-9 is a valid CAS Registry Number.
InChI:InChI=1/C6H10O3.C2H4/c1(5-3-8-5)7-2-6-4-9-6;1-2/h5-6H,1-4H2;1-2H2

2224-15-9 Well-known Company Product Price

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  • TCI America

  • (E0342)  Ethylene Glycol Diglycidyl Ether (so called)  

  • 2224-15-9

  • 25g

  • 260.00CNY

  • Detail
  • TCI America

  • (E0342)  Ethylene Glycol Diglycidyl Ether (so called)  

  • 2224-15-9

  • 500g

  • 925.00CNY

  • Detail

2224-15-9SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 19, 2017

Revision Date: Aug 19, 2017

1.Identification

1.1 GHS Product identifier

Product name Ethylene glycol diglycidyl ether

1.2 Other means of identification

Product number -
Other names 1,2-bis-oxiranylmethoxy-ethane

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Adsorbents and absorbents
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:2224-15-9 SDS

2224-15-9Synthetic route

ethylene glycol
107-21-1

ethylene glycol

epichlorohydrin
106-89-8

epichlorohydrin

ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

Conditions
ConditionsYield
With tetrabutyl-ammonium chloride; water; sodium hydroxide at 40℃; for 0.75h;89%
With fluoroboric acid; trifluorormethanesulfonic acid; boron trifluoride at 40 - 65℃; for 5h; Temperature; Reagent/catalyst; Sonication; Inert atmosphere; Molecular sieve; Large scale;55.7%
With potassium hydroxide; benzyltrioctylammonium chloride at 40℃; for 0.75h;54%
1,10-Dichloro-4,7-dioxa-2,9-decanediol
13078-45-0

1,10-Dichloro-4,7-dioxa-2,9-decanediol

ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

Conditions
ConditionsYield
With sodium hydroxide Dehydrochlorination;40 g
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

tert-butyl glycidyl ether
7580-85-0

tert-butyl glycidyl ether

C14H28O6

C14H28O6

Conditions
ConditionsYield
With boron trifluoride diethyl etherate at 80℃; for 3h;99.3%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

Ethyl 1H,1H-perfluorooctanoxyacetate
134918-67-5

Ethyl 1H,1H-perfluorooctanoxyacetate

1,1-dimethylhydrazine
57-14-7

1,1-dimethylhydrazine

N,N,N',N'-Tetramethyl-4,7-dioxa-2,9-dihydroxy-1,10-decanediamine-N,N'-bis<(1H,1H-perfluorooctanoxyacetyl)imide>

N,N,N',N'-Tetramethyl-4,7-dioxa-2,9-dihydroxy-1,10-decanediamine-N,N'-bis<(1H,1H-perfluorooctanoxyacetyl)imide>

Conditions
ConditionsYield
In methanol Heating;99%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

methyl 2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonanoate
26131-32-8

methyl 2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonanoate

1,1-dimethylhydrazine
57-14-7

1,1-dimethylhydrazine

N,N,N',N'-Tetramethyl-4,7-dioxa-2,9-dihydroxy-1,10-decanediamine-N,N'-bis<(perfluoro-2,5-dimethyl-3,6-dioxanonanoyl)imide>

N,N,N',N'-Tetramethyl-4,7-dioxa-2,9-dihydroxy-1,10-decanediamine-N,N'-bis<(perfluoro-2,5-dimethyl-3,6-dioxanonanoyl)imide>

Conditions
ConditionsYield
In methanol Heating;96%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

Methyl perfluoro-2,5,8,11-tetramethyl-3,6,9,12-tetraoxapentadecanoate
133609-46-8

Methyl perfluoro-2,5,8,11-tetramethyl-3,6,9,12-tetraoxapentadecanoate

1,1-dimethylhydrazine
57-14-7

1,1-dimethylhydrazine

N,N,N',N'-Tetramethyl-4,7-dioxa-2,9-dihydroxy-1,10-decanediamine-N,N'-bis<(perfluoro-2,5,8,11-tetramethyl-3,6,9,12-tetraoxapentadecanoyl)imide>

N,N,N',N'-Tetramethyl-4,7-dioxa-2,9-dihydroxy-1,10-decanediamine-N,N'-bis<(perfluoro-2,5,8,11-tetramethyl-3,6,9,12-tetraoxapentadecanoyl)imide>

Conditions
ConditionsYield
In methanol Heating;96%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

carbon dioxide
124-38-9

carbon dioxide

4-((2-((2-oxo-1,3-dioxolan-4-yl)methoxy)ethoxy)methyl)-1,3-dioxolan-2-one

4-((2-((2-oxo-1,3-dioxolan-4-yl)methoxy)ethoxy)methyl)-1,3-dioxolan-2-one

Conditions
ConditionsYield
With tetrabutylammomium bromide at 110℃; under 7500.75 Torr; for 3h;94%
With C42H44N8O6Zn(2+)*2Cl(1-) In neat (no solvent) at 100℃; under 750.075 Torr; for 24h; Kinetics; Pressure; Temperature; Autoclave;94.5%
With C44H20AlCl9N4; bis(triphenylphosphine)iminium chloride In neat (no solvent) at 120℃; under 22502.3 Torr; for 1h; Autoclave;
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

Methyl perfluoro-2,5,8-trimethyl-3,6,9-trioxadodecanoate
39187-47-8

Methyl perfluoro-2,5,8-trimethyl-3,6,9-trioxadodecanoate

1,1-dimethylhydrazine
57-14-7

1,1-dimethylhydrazine

N,N,N',N'-Tetramethyl-4,7-dioxa-2,9-dihydroxy-1,10-decanediamine-N,N'-bis<(perfluoro-2,5,8-trimethyl-3,6,9-trioxadodecanoyl)imide>

N,N,N',N'-Tetramethyl-4,7-dioxa-2,9-dihydroxy-1,10-decanediamine-N,N'-bis<(perfluoro-2,5,8-trimethyl-3,6,9-trioxadodecanoyl)imide>

Conditions
ConditionsYield
In methanol Heating;94%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

diethylene glycol mono(tert-butyl)ether
110-09-8

diethylene glycol mono(tert-butyl)ether

C16H32O7

C16H32O7

Conditions
ConditionsYield
With Amberlyst-15 resin at 70℃; for 5h;93.2%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

methyl undecafluoro-2-methyl-3-oxahexanoate
13140-34-6

methyl undecafluoro-2-methyl-3-oxahexanoate

1,1-dimethylhydrazine
57-14-7

1,1-dimethylhydrazine

N,N,N',N'-Tetramethyl-4,7-dioxa-2,9-dihydroxy-1,10-decanediamine-N,N'-bis<(perfluoro-2-methyl-3-oxahexanoyl)imide>

N,N,N',N'-Tetramethyl-4,7-dioxa-2,9-dihydroxy-1,10-decanediamine-N,N'-bis<(perfluoro-2-methyl-3-oxahexanoyl)imide>

Conditions
ConditionsYield
In methanol Heating;92%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

1-t-Butoxycarbonylpiperazine
57260-71-6

1-t-Butoxycarbonylpiperazine

ethylene glycol di<2-hydroxy-3-(N'-tert-butoxycarbonylpiperazinyl)>propyl ether
158328-41-7

ethylene glycol di<2-hydroxy-3-(N'-tert-butoxycarbonylpiperazinyl)>propyl ether

Conditions
ConditionsYield
In chloroform for 24h; Heating;91%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

ethane-1,2-dithiol
540-63-6

ethane-1,2-dithiol

C10H20O4S2
1273318-54-9

C10H20O4S2

Conditions
ConditionsYield
With N-benzyl-trimethylammonium hydroxide at 0℃; for 0.5h; Neat (no solvent); regiospecific reaction;90%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

(3-chloropropyl)triethoxysilane
5089-70-3

(3-chloropropyl)triethoxysilane

2,5-Dimercapto-1,3,4-thiadiazole
1072-71-5

2,5-Dimercapto-1,3,4-thiadiazole

C19H36N2O7S3Si

C19H36N2O7S3Si

Conditions
ConditionsYield
Stage #1: ethylene glycol diglycidyl ether; 2,5-Dimercapto-1,3,4-thiadiazole In methanol at 60℃; for 18h;
Stage #2: With sodium methylate In methanol at 20℃; for 0.5h;
Stage #3: (3-chloropropyl)triethoxysilane In methanol at 70℃; for 12h;
90%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

hexan-1-amine
111-26-2

hexan-1-amine

Bistriethylene glycol
92237-82-6

Bistriethylene glycol

Conditions
ConditionsYield
at 120℃; for 4h;82%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

Trimethylenediamine
109-76-2

Trimethylenediamine

1,4-dioxa-8,12-diaza-cyclopentadecane-6,14-diol

1,4-dioxa-8,12-diaza-cyclopentadecane-6,14-diol

Conditions
ConditionsYield
With sodium hydride In water Cycloaddition; Heating;82%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

N,N'-dibenzyl-1,3-diaminopropane
10239-34-6

N,N'-dibenzyl-1,3-diaminopropane

8,11-dibenzyl-1,4-dioxa-8,11-diaza-cyclotetradecane-6,13-diol

8,11-dibenzyl-1,4-dioxa-8,11-diaza-cyclotetradecane-6,13-diol

Conditions
ConditionsYield
With sodium hydride In water Cycloaddition; Heating;80%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

C8H16N6O4

C8H16N6O4

Conditions
ConditionsYield
With sodium azide; ammonium chloride In methanol; water at 80℃; for 24h;80%
With sodium azide In methanol; water at 80℃;
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

phenyl isocyanate
103-71-9

phenyl isocyanate

1,6-bis(3-phenyloxazolidin-2-on-5-yl)-2,5-dioxahexane

1,6-bis(3-phenyloxazolidin-2-on-5-yl)-2,5-dioxahexane

Conditions
ConditionsYield
Stage #1: ethylene glycol diglycidyl ether With Tributylphosphine oxide; lithium bromide In toluene for 2h; Heating;
Stage #2: phenyl isocyanate In toluene for 12h; Heating; Further stages.;
78%
carbon disulfide
75-15-0

carbon disulfide

ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

1,6-bis(oxathiolane-2-thione-5-yl)-2,5-dioxahexane

1,6-bis(oxathiolane-2-thione-5-yl)-2,5-dioxahexane

Conditions
ConditionsYield
Stage #1: ethylene glycol diglycidyl ether With lithium bromide In dichloromethane for 2h; Heating;
Stage #2: carbon disulfide In dichloromethane for 10h; Heating; Further stages.;
76%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

1,4,10,13-tetraoxa-7,16-diazacyclooctadecane
23978-55-4

1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

A

3,10,23,29-tetrahydroxy-5,8,15,18,25,28,35,38,43,46,51,54-dodecaoxa-1,12,21,32-tetraazatricyclo<30.30.8.812,21>hexapentacontane
119017-33-3

3,10,23,29-tetrahydroxy-5,8,15,18,25,28,35,38,43,46,51,54-dodecaoxa-1,12,21,32-tetraazatricyclo<30.30.8.812,21>hexapentacontane

B

3,10-dihydroxy-5,8,15,18,23,26-hexaoxa-1,12-diazabicyclo<10.8.8>octacosane
117536-17-1

3,10-dihydroxy-5,8,15,18,23,26-hexaoxa-1,12-diazabicyclo<10.8.8>octacosane

Conditions
ConditionsYield
In tetrahydrofuran; ethanol for 10h; Heating;A 1%
B 69%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

1,4,10,13-tetraoxa-7,16-diazacyclooctadecane
23978-55-4

1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

3,10-dihydroxy-5,8,15,18,23,26-hexaoxa-1,12-diazabicyclo<10.8.8>octacosane

3,10-dihydroxy-5,8,15,18,23,26-hexaoxa-1,12-diazabicyclo<10.8.8>octacosane

Conditions
ConditionsYield
In tetrahydrofuran; ethanol Heating;69%
carbon disulfide
75-15-0

carbon disulfide

ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

phenyl isocyanate
103-71-9

phenyl isocyanate

5-(6-oxathiolan-2-thione-2,5-dioxahexan-5-yl)-3-phenyloxazolidin-2-one

5-(6-oxathiolan-2-thione-2,5-dioxahexan-5-yl)-3-phenyloxazolidin-2-one

Conditions
ConditionsYield
Stage #1: ethylene glycol diglycidyl ether With lithium bromide In tetrahydrofuran for 0.5h; Inert atmosphere; Reflux;
Stage #2: phenyl isocyanate In tetrahydrofuran Inert atmosphere; Reflux;
Stage #3: carbon disulfide In tetrahydrofuran at 20℃; for 7h; Inert atmosphere;
67%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

ethylamine
75-04-7

ethylamine

1-Ethylamino-3-[2-(3-ethylamino-2-hydroxy-propoxy)-ethoxy]-propan-2-ol
92237-85-9

1-Ethylamino-3-[2-(3-ethylamino-2-hydroxy-propoxy)-ethoxy]-propan-2-ol

Conditions
ConditionsYield
In water for 50h; Ambient temperature;64%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

1,10-diamino-4,7-dioxadecan-2,9-diol
4454-09-5

1,10-diamino-4,7-dioxadecan-2,9-diol

Conditions
ConditionsYield
With ammonia for 50h; Ambient temperature;63%
carbon disulfide
75-15-0

carbon disulfide

ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

5-[6-oxiran-2,5-dioxahexan]-1,3-oxathiolane-2-thione

5-[6-oxiran-2,5-dioxahexan]-1,3-oxathiolane-2-thione

Conditions
ConditionsYield
With lithium bromide In dichloromethane for 5h; Inert atmosphere; Reflux; regioselective reaction;58%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

1,10-Dichloro-4,7-dioxa-2,9-decanediol
13078-45-0

1,10-Dichloro-4,7-dioxa-2,9-decanediol

Conditions
ConditionsYield
With hydrogenchloride56%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

phenyl isocyanate
103-71-9

phenyl isocyanate

5-(6-oxiran-2,5-dioxahexan-5-yl)-3-phenyloxazolidin-2-one

5-(6-oxiran-2,5-dioxahexan-5-yl)-3-phenyloxazolidin-2-one

Conditions
ConditionsYield
Stage #1: ethylene glycol diglycidyl ether With lithium bromide In tetrahydrofuran for 0.5h; Inert atmosphere; Reflux;
Stage #2: phenyl isocyanate In tetrahydrofuran for 6h; Inert atmosphere; Reflux;
54%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

1,4,7-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane
175854-39-4

1,4,7-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane

C54H102N8O16

C54H102N8O16

Conditions
ConditionsYield
In ethanol for 120h; Heating;53.2%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

Kryptofix 21
31249-95-3

Kryptofix 21

3,10-dihydroxy-5,8,13,18,23-pentaoxa-1,12-diazabicyclo<10.8.5>pentacosane
129940-62-1

3,10-dihydroxy-5,8,13,18,23-pentaoxa-1,12-diazabicyclo<10.8.5>pentacosane

Conditions
ConditionsYield
In tetrahydrofuran; ethanol for 10h; Heating;51%
2,3-dichlorotetrahydrofuran
3511-19-1

2,3-dichlorotetrahydrofuran

ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

1,12-di(3-chloro-2-tetrahydrofuryl)-3,10-dichloro-1,5,8,12-tetraoxadodecane
137675-79-7

1,12-di(3-chloro-2-tetrahydrofuryl)-3,10-dichloro-1,5,8,12-tetraoxadodecane

Conditions
ConditionsYield
With zinc(II) chloride In tetrachloromethane at 40℃; for 1h;50.7%
ethylene glycol diglycidyl ether
2224-15-9

ethylene glycol diglycidyl ether

diaza[12]crown-4
294-92-8

diaza[12]crown-4

A

3,10,20,27-tetrahydroxy-5,8,15,22,25,32,37,42-octaoxa-1,12,18,29-tetraazatricyclo<27.27.5.51,29>tetratetracontane
113769-01-0

3,10,20,27-tetrahydroxy-5,8,15,22,25,32,37,42-octaoxa-1,12,18,29-tetraazatricyclo<27.27.5.51,29>tetratetracontane

B

meso-3,10-dihydroxy-5,8,15,20-tetraoxa-1,12-diazabicyclo<10.5.5>docosane
113769-00-9

meso-3,10-dihydroxy-5,8,15,20-tetraoxa-1,12-diazabicyclo<10.5.5>docosane

Conditions
ConditionsYield
In tetrahydrofuran; ethanol for 10h; Heating;A 14%
B 46%
In tetrahydrofuran; ethanol for 5h; Heating;A 37.5%
B 22.5%
In tetrahydrofuran; ethanol for 10h; Heating;

2224-15-9Relevant articles and documents

-

Cohen,Haas

, p. 1733 (1953)

-

Quaternary ammonium salt polymer and preparation method and application thereof

-

Paragraph 0061-0062, (2020/05/29)

The invention provides a quaternary ammonium salt polymer and a preparation method and application thereof. The structure of the quaternary ammonium salt polymer contains a hydrophilic group and adjustable hydrophilic/hydrophobic groups such as PPG and PAG. With high surface tension, the quaternary ammonium salt polymer can effectively separate miscellaneous oil wrapping metal cuttings and enablesthe miscellaneous oil to float above a metal processing aqueous solution, so demulsification can be effectively realized, the surface tension of the solution is increased, and the oil floats to a liquid level; and compared with an existing sedimentation additive for a metal working fluid, the quaternary ammonium salt polymer can effectively settle particles in the metal working fluid, and has good application prospects.

Synthesis method of ethylene glycol diglycidyl ether

-

Paragraph 0014; 0015; 0016; 0017; 0018; 0019, (2017/07/21)

The invention relates to a synthesis method of ethylene glycol diglycidyl ether. According to the method, ethylene glycol and epoxy chloropropane are used as raw materials; argon gas is continuously introduced; ring-opening reaction is performed under the combined action of ultrasonic waves and a ternary composite catalyst. A 5A molecular sieve and the ternary composite catalyst are combined, so that the catalyst dosage is greatly reduced; the reaction progress is accelerated; the method is suitable for industrial large-scale production. After the reaction is completed, the temperature is lowered; the mixture and liquid alkaline take ring-closure reaction under the effects of solvent methylbenzene and a 3A molecular sieve supported phase transfer catalyst; the 3A molecular sieve supported phase transfer catalyst has high reaction activity; after the reaction is completed, water washing is very smooth; after methylbenzene and water are removed from a crude product, the ethylene glycol diglycidyl ether with high epoxide value is obtained, wherein the epoxide value can reach 0.78. Compared with the prior art, the synthesis method has the advantages that the selectivity is high; side reactions are few; the reaction effect is good; the yield is high; the product quality is the best; the cost performance is high.

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