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Cas Database

22564-57-4

22564-57-4

Identification

  • Product Name:Phosphoric acid, bis(2-chloroethyl) phenyl ester

  • CAS Number: 22564-57-4

  • EINECS:

  • Molecular Weight:299.091

  • Molecular Formula: C10H13Cl2O4P

  • HS Code:

  • Mol File:22564-57-4.mol

Synonyms:

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Relevant articles and documentsAll total 1 Articles be found

Synthesis of phosphorus derivatives from 1,3-dioxolan-2-one

Ilia, Gheorghe,Bora, Alina,Iliescu, Smaranda,Popa, Adriana,Dehelean, Gheorghe

, p. 2491 - 2496 (2003)

A new route for the synthesis of some mixed organic phosphorus compounds from 1,3-dioxolan-2-one is reported. By heating a mixture of phosphorus-chlorine derivatives and 1,3-dioxolan-2-one in the presence of a catalyst, mixed phosphorus derivatives having 2-chloroethyl ester groups could be obtained. A wide range of phosphorus derivatives can be obtained using this method.

Process route upstream and downstream products

Process route

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

chlorophosphoric acid diphenyl ester
2524-64-3

chlorophosphoric acid diphenyl ester

bis(2-chloroethyl) phenyl phosphate
22564-57-4

bis(2-chloroethyl) phenyl phosphate

phosphoric acid triphenyl ester
115-86-6

phosphoric acid triphenyl ester

2-chloroethyl diphenyl phosphate
5314-06-7

2-chloroethyl diphenyl phosphate

Conditions
Conditions Yield
With guanidine hydrogen carbonate; at 120 ℃; for 3h;
59%
3%
3%
With lithium fluoride; at 170 ℃; for 3h;
20%
35%
10%
With lithium chloride; at 170 ℃; for 3h;
10%
28%
18%
O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

bis(2-chloroethyl) phenyl phosphate
22564-57-4

bis(2-chloroethyl) phenyl phosphate

Conditions
Conditions Yield
With titanium tetrachloride;
2-chloro-ethanol
107-07-3

2-chloro-ethanol

bis(2-chloroethyl) phenyl phosphate
22564-57-4

bis(2-chloroethyl) phenyl phosphate

Conditions
Conditions Yield
With air; trichlorophosphate; phenol;
O-phenyl phosphorodichloridate
770-12-7

O-phenyl phosphorodichloridate

2-chloro-ethanol
107-07-3

2-chloro-ethanol

bis(2-chloroethyl) phenyl phosphate
22564-57-4

bis(2-chloroethyl) phenyl phosphate

Conditions
Conditions Yield
With pyridine; benzene;
bis(2-chloroethyl) phenyl phosphate
22564-57-4

bis(2-chloroethyl) phenyl phosphate

Conditions
Conditions Yield
C6H5OPOCl2, Oxiran;

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