22877-03-8

Basic information

• Product Name: 4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-[3-(acetyloxy)-4-methoxyphenyl]-
• CAS NO: 22877-03-8
• Molecular Formula: C20H16O7
• Molecular Weight: 368.343
• Mol File: 22877-03-8.mol
• Article Data: 1

Chemical Properties

• CAS DataBase Reference: 4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-[3-(acetyloxy)-4-methoxyphenyl]-(CAS DataBase Reference)
• NIST Chemistry Reference: 4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-[3-(acetyloxy)-4-methoxyphenyl]-(22877-03-8)
• EPA Substance Registry System: 4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-[3-(acetyloxy)-4-methoxyphenyl]-(22877-03-8)

Safety Data

• Hazardous Substances Data: 22877-03-8(Hazardous Substances Data)

Upstream product

• 20575-57-9 calycosin 
• 108-24-7 acetic anhydride 
• 108-46-3 recorcinol 
• 1131-94-8 homoisovanillic acid 

Downstream Products

• 20633-67-4 calycosin-7-O-β-D-glucopyranoside 

Relevant articles and documents

A method of chemical synthesis mao Ruiyi flavonoid (by machine translation)

The invention relates to a method for preparing mao Ruiyi flavonoid, comprises the following steps: to resorcinol and 3 - hydroxy -4 - methoxy acetic acid (as the starting material, to make the 3 ', 7 - dihydroxy -4' - methoxyisoflavone, then through the acetylation reaction to obtain the double-b acylated product 3 ', 7 - acetoxy -4' - methoxyisoflavone; selective shall get rid of the 7 bit on the hydroxy protecting group and gets the 7 - hydroxy -3 '- acetoxy -4' - methoxyisoflavone; the 7 position hydroxy generating glycosidic bond to obtain 3 '- acetoxy -4' - methoxyisoflavone - 7 - O - beta - D - tetra-substituted-based glucoside, finally through complete hydrolysis, removing the protecting group to obtain mao Ruiyi flavonoid, namely calycosin - 7 - O - beta - D - glucoside. The invention develops mao Ruiyi flavonoid glycoside of chemical synthesis method, this synthetic route raw materials are easy, and the cost is low, mild reaction conditions. (by machine translation)