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4107-65-7

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4107-65-7 Usage

Chemical Properties

white to slightly yellow crystalline powder

Uses

2,4-Dimethoxybenzonitrile was used in the preparation of 2,4-dimethoxybenzylamine.

Check Digit Verification of cas no

The CAS Registry Mumber 4107-65-7 includes 7 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 4 digits, 4,1,0 and 7 respectively; the second part has 2 digits, 6 and 5 respectively.
Calculate Digit Verification of CAS Registry Number 4107-65:
(6*4)+(5*1)+(4*0)+(3*7)+(2*6)+(1*5)=67
67 % 10 = 7
So 4107-65-7 is a valid CAS Registry Number.
InChI:InChI=1/C9H9NO2/c1-11-8-4-3-7(6-10)9(5-8)12-2/h3-5H,1-2H3

4107-65-7 Well-known Company Product Price

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  • Alfa Aesar

  • (B24621)  2,4-Dimethoxybenzonitrile, 99%   

  • 4107-65-7

  • 5g

  • 186.0CNY

  • Detail
  • Alfa Aesar

  • (B24621)  2,4-Dimethoxybenzonitrile, 99%   

  • 4107-65-7

  • 25g

  • 729.0CNY

  • Detail
  • Alfa Aesar

  • (B24621)  2,4-Dimethoxybenzonitrile, 99%   

  • 4107-65-7

  • 100g

  • 2469.0CNY

  • Detail

4107-65-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 11, 2017

Revision Date: Aug 11, 2017

1.Identification

1.1 GHS Product identifier

Product name 2,4-Dimethoxybenzonitrile

1.2 Other means of identification

Product number -
Other names 2,4,8-TRIMETHYL-1,2,3,4-TETRAHYDRO-QUINOLINE

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:4107-65-7 SDS

4107-65-7Relevant articles and documents

Envirocat EPZG(R), a new catalyst for the conversion of aldoximes into nitriles

Bandgar,Jagtap,Ghodeshwar,Wadgaonkar

, p. 2993 - 2998 (1995)

The conversion of aldoximes into nitriles was carried out at 100°C in the absence of a solvent using Envirocat EPZG(R) as a new solid supported catalyst.

SO2F2-mediated oxidation of primary and tertiary amines with 30% aqueous H2O2 solution

Liao, Xudong,Zhou, Yi,Ai, Chengmei,Ye, Cuijiao,Chen, Guanghui,Yan, Zhaohua,Lin, Sen

supporting information, (2021/11/01)

A highly efficient and selective oxidation of primary and tertiary amines employing SO2F2/H2O2/base system was described. Anilines were converted to the corresponding azoxybenzenes, while primary benzylamines were transformed into nitriles and secondary benzylamines were rearranged to amides. For tertiary amine substrates quinolines, isoquinolines and pyridines, their oxidation products were the corresponding N-oxides. The reaction conditions are very mild and just involve SO2F2, amines, 30% aqueous H2O2 solution, and inorganic base at room temperature. One unique advantage is that this oxidation system is just composed of inexpensive inorganic compounds without the use of any metal and organic compounds.

Acceptorless dehydrogenation of amines to nitriles catalyzed by N-heterocyclic carbene-nitrogen-phosphine chelated bimetallic ruthenium (II) complex

Chen, Hua,Fu, Haiyan,Ji, Li,Li, Ruixiang,Nie, Xufeng,Zheng, Yanling

, p. 378 - 385 (2020/10/02)

We have developed a clean, atom-economical and environmentally friendly route for acceptorless dehydrogenation of amines to nitriles by combining a new dual N-heterocyclic carbene-nitrogen-phosphine ligand R(CNP)2 (R = o-xylyl) with a ruthenium precursor [RuCl2(η6-C6H6)]2. In this system, the electronic and steric factors of amines had a negligible influence on the reaction and a broad range of functional groups were well tolerated. All of the investigated amines could be converted to nitriles in good yield of up to 99% with excellent selectivity. The unprecedented catalytic performance of this system is attributed to the synergistic effect of two ruthenium centers chelated by R(CNP)2 and a plausible reaction mechanism is proposed according to the active species found via in situ NMR and HRMS.

Method for converting aromatic aldehyde into aromatic nitrile by using sulfur powder promoted inorganic ammonium as nitrogen source (by machine translation)

-

Paragraph 0046; 0047, (2020/09/12)

The invention discloses a method for converting aromatic aldehyde into aromatic nitrile. The method is conversion of high yield of aromatic aldehyde one-pot reaction of sulfur powder promoted inorganic ammonium as a nitrogen source into aromatic nitrile. The method has the advantages of no need of metal participation, no need of strong oxide, compatibility of reaction to air, easiness in amplification to a gram scale and the like, and overcomes the problems of harsh reaction conditions, complex operation, low functional group compatibility and the like in the prior art. (by machine translation)

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