4467-90-7Relevant articles and documents
An efficient method for the synthesis of α-arylated nitroalkanes and α-arylated hydroximoyl chlorides mediated by AlCl3
Tu, Zhijay,Rama Raju,Liou, Tzuo-Rung,Kavala, Veerababurao,Kuo, Chun-Wei,Jang, Yaochung,Shih, Yu-Hsuan,Wang, Chun-Chao,Yao, Ching-Fa
experimental part, p. 2436 - 2442 (2009/07/25)
Friedel-Crafts alkylation of various arenes/heteroarenes to β-nitrostyrenes mediated by aluminum chloride is described. The interesting feature of this methodology pertain the formation of different products by tuning the reaction temperature. α-Arylated
A facile one-pot preparation of isothiocyanates from aldoximes
Kim, Jae Nyoung,Jung, Keum Shin,Lee, Hong Jung,Son, Ji Suk
, p. 1597 - 1598 (2007/10/03)
Isothiocyanates 2a-l were prepared in excellent yields in a one-pot reaction from aldoxime derivatives 1a-l by successive treatment of aldoxime with N-chlorosuccinimide (NCS), thiourea, and triethylamine. The use of HCl/DMF/Oxone system in the reaction instead of NCS was equally effective.