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Cas Database

4560-58-1

4560-58-1

Identification

  • Product Name:(4R)-4-[(3S,5R,8R,9S,10S,13R,14S,17R)-3-hydroxy-10,13-dimethyl-12-oxo-1,2,3,4,5,6,7,8,9,11,14,15,16,17-tetradecahydrocyclopenta[a]phenanthren-17-yl]pentanoic acid

  • CAS Number: 4560-58-1

  • EINECS:

  • Molecular Weight:390.563

  • Molecular Formula: C24H38O4

  • HS Code:

  • Mol File:4560-58-1.mol

Synonyms:

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Safety information and MSDS view more

  • Signal Word:no data available

  • Hazard Statement:no data available

  • First-aid measures: General adviceConsult a physician. Show this safety data sheet to the doctor in attendance.If inhaled If breathed in, move person into fresh air. If not breathing, give artificial respiration. Consult a physician. In case of skin contact Wash off with soap and plenty of water. Consult a physician. In case of eye contact Rinse thoroughly with plenty of water for at least 15 minutes and consult a physician. If swallowed Never give anything by mouth to an unconscious person. Rinse mouth with water. Consult a physician.

  • Fire-fighting measures: Suitable extinguishing media Use water spray, alcohol-resistant foam, dry chemical or carbon dioxide. Wear self-contained breathing apparatus for firefighting if necessary.

  • Accidental release measures: Use personal protective equipment. Avoid dust formation. Avoid breathing vapours, mist or gas. Ensure adequate ventilation. Evacuate personnel to safe areas. Avoid breathing dust. For personal protection see section 8. Prevent further leakage or spillage if safe to do so. Do not let product enter drains. Discharge into the environment must be avoided. Pick up and arrange disposal. Sweep up and shovel. Keep in suitable, closed containers for disposal.

  • Handling and storage: Avoid contact with skin and eyes. Avoid formation of dust and aerosols. Avoid exposure - obtain special instructions before use.Provide appropriate exhaust ventilation at places where dust is formed. For precautions see section 2.2. Store in cool place. Keep container tightly closed in a dry and well-ventilated place.

  • Exposure controls/personal protection:Occupational Exposure limit valuesBiological limit values Handle in accordance with good industrial hygiene and safety practice. Wash hands before breaks and at the end of workday. Eye/face protection Safety glasses with side-shields conforming to EN166. Use equipment for eye protection tested and approved under appropriate government standards such as NIOSH (US) or EN 166(EU). Skin protection Wear impervious clothing. The type of protective equipment must be selected according to the concentration and amount of the dangerous substance at the specific workplace. Handle with gloves. Gloves must be inspected prior to use. Use proper glove removal technique(without touching glove's outer surface) to avoid skin contact with this product. Dispose of contaminated gloves after use in accordance with applicable laws and good laboratory practices. Wash and dry hands. The selected protective gloves have to satisfy the specifications of EU Directive 89/686/EEC and the standard EN 374 derived from it. Respiratory protection Wear dust mask when handling large quantities. Thermal hazards

Supplier and reference price

  • Manufacture/Brand
  • Product Description
  • Packaging
  • Price
  • Delivery
  • Purchase
  • Manufacture/Brand:American Custom Chemicals Corporation
  • Product Description:3-BETA-HYDROXY-12-OXO-5-BETA-CHOLANOIC ACID 95.00%
  • Packaging:5MG
  • Price:$ 500.72
  • Delivery:In stock
  • Buy Now

Relevant articles and documentsAll total 2 Articles be found

-

Dutcher,Wintersteiner

, p. 1992,1998 (1939)

-

synthetic bile acid preparation

-

Paragraph 0109-0111, (2015/09/28)

no abstract published

SYNTHETIC BILE ACID COMPOSITIONS AND METHODS

-

Page/Page column 48, (2012/03/09)

Bile acids and related compositions and methods of synthesis and use. More specifically, deoxycholic acid and related compositions, said compositions being free of all moieties of animal origin and free of pyrogenic moieties.

Process route upstream and downstream products

Process route

3α-hydroxy-12-semicarbazono-5β-cholanoic acid-(24)

3α-hydroxy-12-semicarbazono-5β-cholanoic acid-(24)

sodium ethanolate
141-52-6

sodium ethanolate

Lithocholic acid
434-13-9

Lithocholic acid

12-oxolithocholic acid
5130-29-0,83830-81-3

12-oxolithocholic acid

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)
4560-58-1,83830-81-3

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)

Conditions
Conditions Yield
at 200 ℃;
3,12-disemicarbazono-5β-cholanoic acid-(24)

3,12-disemicarbazono-5β-cholanoic acid-(24)

sodium ethanolate
141-52-6

sodium ethanolate

cholanic acid
25312-65-6

cholanic acid

12-oxolithocholic acid
5130-29-0,83830-81-3

12-oxolithocholic acid

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)
4560-58-1,83830-81-3

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)

Conditions
Conditions Yield
at 200 ℃;
methyl 3β-hydroxy-5β-cholane-12-one-24-oate acetate
122441-64-9

methyl 3β-hydroxy-5β-cholane-12-one-24-oate acetate

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)
4560-58-1,83830-81-3

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)

Conditions
Conditions Yield
With methanol; sodium hydroxide; at 20 ℃; for 2h;
With sodium hydroxide; In methanol; at 20 ℃; for 2h;
methyl 3β-hydroxy-5β-chol-9(11)-ene-24-oate acetate
881023-82-1

methyl 3β-hydroxy-5β-chol-9(11)-ene-24-oate acetate

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)
4560-58-1,83830-81-3

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)

Conditions
Conditions Yield
Multi-step reaction with 3 steps
1: chromium(VI) oxide; acetic acid / 60 °C
2: hydrogen / palladium 10% on activated carbon / ethyl acetate / 16 h / 2585.81 Torr
3: sodium hydroxide; methanol / 2 h / 20 °C
With chromium(VI) oxide; methanol; hydrogen; acetic acid; sodium hydroxide; palladium 10% on activated carbon; In ethyl acetate;
Multi-step reaction with 3 steps
1: chromium(VI) oxide / acetic acid / 60 °C
2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 16 h / 3620.13 Torr / Autoclave
3: sodium hydroxide / methanol / 2 h / 20 °C
With chromium(VI) oxide; palladium 10% on activated carbon; hydrogen; sodium hydroxide; In methanol; acetic acid; ethyl acetate;
methyl 3β-hydroxy-5β-chol-9(11)-ene-12-one-24-oate acetate
4472-02-0

methyl 3β-hydroxy-5β-chol-9(11)-ene-12-one-24-oate acetate

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)
4560-58-1,83830-81-3

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 16 h / 2585.81 Torr
2: sodium hydroxide; methanol / 2 h / 20 °C
With methanol; hydrogen; sodium hydroxide; palladium 10% on activated carbon; In ethyl acetate;
Multi-step reaction with 2 steps
1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 16 h / 3620.13 Torr / Autoclave
2: sodium hydroxide / methanol / 2 h / 20 °C
With palladium 10% on activated carbon; hydrogen; sodium hydroxide; In methanol; ethyl acetate;
3,12-dioxo-7-deoxycholic acid
2958-05-6

3,12-dioxo-7-deoxycholic acid

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)
4560-58-1,83830-81-3

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)

Conditions
Conditions Yield
With hydrogen bromide; acetic acid; platinum; Hydrogenation;
4β-bromo-3,12-dioxo-5β-cholanoic acid-(24)
26425-57-0

4β-bromo-3,12-dioxo-5β-cholanoic acid-(24)

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)
4560-58-1,83830-81-3

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)

Conditions
Conditions Yield
Multi-step reaction with 4 steps
1: acetic acid
2: diethyl ether; methanol
3: Raney nickel; methanol / Hydrogenation
4: methanol. KOH-solution
With methanol; potassium hydroxide; diethyl ether; nickel; acetic acid;
Multi-step reaction with 4 steps
1: pyridine
2: diethyl ether; methanol
3: Raney nickel; methanol / Hydrogenation
4: methanol. KOH-solution
With pyridine; methanol; potassium hydroxide; diethyl ether; nickel;
3β-hydroxy-12-oxo-5β-cholan-24-oic acid methyl ester
18069-51-7

3β-hydroxy-12-oxo-5β-cholan-24-oic acid methyl ester

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)
4560-58-1,83830-81-3

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)

Conditions
Conditions Yield
With potassium hydroxide;
3,12-dioxochol-4-ene-24-oic acid
26425-68-3

3,12-dioxochol-4-ene-24-oic acid

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)
4560-58-1,83830-81-3

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)

Conditions
Conditions Yield
Multi-step reaction with 3 steps
1: diethyl ether; methanol
2: Raney nickel; methanol / Hydrogenation
3: methanol. KOH-solution
With methanol; potassium hydroxide; diethyl ether; nickel;
methyl 3,12-dioxo-5β-chol-4(5)-en-24-oate
80322-20-9

methyl 3,12-dioxo-5β-chol-4(5)-en-24-oate

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)
4560-58-1,83830-81-3

3β-hydroxy-12-oxo-5β-cholanoic acid-(24)

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: Raney nickel; methanol / Hydrogenation
2: methanol. KOH-solution
With methanol; potassium hydroxide; nickel;

Global suppliers and manufacturers

Global( 3) Suppliers
  • Company Name
  • Business Type
  • Contact Tel
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  • Main Products
  • Country
  • Career Henan Chemical Co
  • Business Type:Lab/Research institutions
  • Contact Tel:+86-371-86658258
  • Emails:purchase@coreychem.com
  • Main Products:1
  • Country:China (Mainland)
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