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760212-58-6

760212-58-6

Identification

  • Product Name:1H-Benzimidazole, 1-(4-bromophenyl)-2-phenyl-

  • CAS Number: 760212-58-6

  • EINECS:

  • Molecular Weight:349.23

  • Molecular Formula: C19H13BrN2

  • HS Code:2933990090

  • Mol File:760212-58-6.mol

Synonyms:1-(4-bromophenyl)-2-phenylbenzimidazole;

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Safety information and MSDS view more

  • Signal Word:no data available

  • Hazard Statement:no data available

  • First-aid measures: General adviceConsult a physician. Show this safety data sheet to the doctor in attendance.If inhaled If breathed in, move person into fresh air. If not breathing, give artificial respiration. Consult a physician. In case of skin contact Wash off with soap and plenty of water. Consult a physician. In case of eye contact Rinse thoroughly with plenty of water for at least 15 minutes and consult a physician. If swallowed Never give anything by mouth to an unconscious person. Rinse mouth with water. Consult a physician.

  • Fire-fighting measures: Suitable extinguishing media Use water spray, alcohol-resistant foam, dry chemical or carbon dioxide. Wear self-contained breathing apparatus for firefighting if necessary.

  • Accidental release measures: Use personal protective equipment. Avoid dust formation. Avoid breathing vapours, mist or gas. Ensure adequate ventilation. Evacuate personnel to safe areas. Avoid breathing dust. For personal protection see section 8. Prevent further leakage or spillage if safe to do so. Do not let product enter drains. Discharge into the environment must be avoided. Pick up and arrange disposal. Sweep up and shovel. Keep in suitable, closed containers for disposal.

  • Handling and storage: Avoid contact with skin and eyes. Avoid formation of dust and aerosols. Avoid exposure - obtain special instructions before use.Provide appropriate exhaust ventilation at places where dust is formed. For precautions see section 2.2. Store in cool place. Keep container tightly closed in a dry and well-ventilated place.

  • Exposure controls/personal protection:Occupational Exposure limit valuesBiological limit values Handle in accordance with good industrial hygiene and safety practice. Wash hands before breaks and at the end of workday. Eye/face protection Safety glasses with side-shields conforming to EN166. Use equipment for eye protection tested and approved under appropriate government standards such as NIOSH (US) or EN 166(EU). Skin protection Wear impervious clothing. The type of protective equipment must be selected according to the concentration and amount of the dangerous substance at the specific workplace. Handle with gloves. Gloves must be inspected prior to use. Use proper glove removal technique(without touching glove's outer surface) to avoid skin contact with this product. Dispose of contaminated gloves after use in accordance with applicable laws and good laboratory practices. Wash and dry hands. The selected protective gloves have to satisfy the specifications of EU Directive 89/686/EEC and the standard EN 374 derived from it. Respiratory protection Wear dust mask when handling large quantities. Thermal hazards

Supplier and reference price

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  • Manufacture/Brand:TRC
  • Product Description:1-(4-Bromophenyl)-2-phenyl-1H-benzo[d]imidazole
  • Packaging:100mg
  • Price:$ 75
  • Delivery:In stock
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  • Manufacture/Brand:TCI Chemical
  • Product Description:1-(4-Bromophenyl)-2-phenylbenzimidazole >98.0%(GC)(T)
  • Packaging:1g
  • Price:$ 57
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  • Manufacture/Brand:TCI Chemical
  • Product Description:1-(4-Bromophenyl)-2-phenylbenzimidazole >98.0%(GC)(T)
  • Packaging:5g
  • Price:$ 282
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  • Manufacture/Brand:Crysdot
  • Product Description:1-(4-Bromophenyl)-2-phenyl-1H-benzo[d]imidazole 95+%
  • Packaging:25g
  • Price:$ 302
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  • Manufacture/Brand:Crysdot
  • Product Description:1-(4-Bromophenyl)-2-phenyl-1H-benzo[d]imidazole 95+%
  • Packaging:100g
  • Price:$ 990
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  • Manufacture/Brand:American Custom Chemicals Corporation
  • Product Description:1-(4-BROMOPHENYL)-2-PHENYL-1H-BENZO[D]IMIDAZOLE 95.00%
  • Packaging:5MG
  • Price:$ 504.61
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  • Manufacture/Brand:Ambeed
  • Product Description:1-(4-Bromophenyl)-2-phenyl-1H-benzo[d]imidazole 95%
  • Packaging:100g
  • Price:$ 1014
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  • Manufacture/Brand:Ambeed
  • Product Description:1-(4-Bromophenyl)-2-phenyl-1H-benzo[d]imidazole 95%
  • Packaging:10g
  • Price:$ 160
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  • Manufacture/Brand:Ambeed
  • Product Description:1-(4-Bromophenyl)-2-phenyl-1H-benzo[d]imidazole 95%
  • Packaging:5g
  • Price:$ 96
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  • Manufacture/Brand:Ambeed
  • Product Description:1-(4-Bromophenyl)-2-phenyl-1H-benzo[d]imidazole 95%
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Relevant articles and documentsAll total 15 Articles be found

Transition-Metal-Free Synthesis of 1,2-diphenyl-1H-benzo[d] Imidazole Derivatives from N-phenylbenzimidamides and Cyclohexanones

Lu, Guoqiang,Luo, Nan,Hu, Fangpeng,Ban, Zihui,Zhan, Zhenzhen,Huang, Guo-Sheng

supporting information, p. 487 - 492 (2019/12/12)

A transition-metal-free strategy for the formation of 1,2-diphenyl-1H-benzo[d] imidazoles from N-phenylbenzimidamides and cyclohexanones is introduced. This is the first report on the direct synthesis of 1,2-diphenyl-1H-benzo[d] imidazoles from cyclohexanones and N-phenylbenzimidamides via iodine- promoted oxidative cyclization. Non-aromatic cyclohexanones were smoothly dehydrogenated, and acted as an aryl source using oxygen as a green oxidant. The catalytic use of iodine makes this method quite simple, more economical and convenient. Under optimized conditions, various substituted 1,2-diphenyl-1H-benzo[d] imidazoles were smoothly reacted, and the desired substituted imidazoles were generated with moderate to excellent yields. (Figure presented.).

Substituted 1,3,5-triazine compound, composition and application thereof

-

Paragraph 0221; 0224, (2020/10/16)

The invention discloses a substituted 1,3,5-triazine compound, a composition and application thereof. The 1,3,5-triazine compound shown as a formula I is provided by the invention, can be used as an electron transport material and, can be used as an electron acceptor material. The composition that can be used for preparing an electron transport layer or an electron donor material is used as a mainbody material of an electroluminescent device, so that the prepared electroluminescent device has the advantages of relatively high efficiency, relatively long service lifetime and the like. As the 1,3,5-triazine compound is used as an electron transport layer, the composition used as an electron acceptor material and an electron donor material is adopted to construct a light-emitting layer, andthe prepared electroluminescent device has the advantages of higher efficiency, longer service lifetime and the like.

Bipyridyl derivative and application thereof

-

, (2019/08/06)

The present invention provides a novel compound, which has a structure general formula represented by a formula (I), wherein Ar1 and Ar2 are independently selected from an aromatic hydrocarbon derivative group containing benzimidazoyl, an aromatic hydrocarbon derivative group containing a pyridine group, substituted or unsubstituted C6-C30 aromatic hydrocarbon, and a substituted or unsubstituted C6-C30 fused ring aromatic hydrocarbon group, and R1 and R2 are independently and respectively selected from H, C1-C12 aliphatic hydrocarbon radical, phenyl, substituted phenyl, naphthyl, substituted naphthyl, biphenyl and substituted biphenyl. According to the present invention, the compound has characteristics of stable character, simple preparation process, high luminous efficiency and high carrier mobility, and can be used for the electron transport layer of the electroluminescent element, and the device applying the compound has characteristics of significant driving voltage reducing and current efficiency improving. The formula (I) is defined in the instruction.

Compound for organic optoelectronic device, organic light emitting diode including the same and display including the organic light emitting diode

-

, (2017/02/09)

A compound for an organic optoelectronic device is represented by Chemical Formula 1: and, in Chemical Formula 1, one of Ar1 or Ar2 is a substituted or unsubstituted C6 to C30 aryl group, or a substituted or unsubstituted C3 to C30 heteroaryl group, and the other of Ar1 or Ar2 is a substituent represented by the Chemical Formula 2:

Boron-containig benzopyrenes derivatives, their preparation and organic electroluminescent device (by machine translation)

-

, (2016/10/07)

The present invention relates to a 6-tritolyl-6H-6-bora benzo[cd]pyrene derivative represented by a formula (1), wherein substituents are described in an instruction. The present invention further relates to uses of the compound as an electron transportation material, and an organic electroluminescent device containing the compound. Formula (1).

Process route upstream and downstream products

Process route

N-[2-(4-bromophenyl amino) phenyl] benzamide
760212-57-5

N-[2-(4-bromophenyl amino) phenyl] benzamide

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene
760212-58-6

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene

Conditions
Conditions Yield
With toluene-4-sulfonic acid; In 5,5-dimethyl-1,3-cyclohexadiene; at 150 ℃; for 12h;
79%
With toluene-4-sulfonic acid; In xylene; for 3h; Heating / reflux;
52%
With toluene-4-sulfonic acid; In xylene; for 3h; Heating / reflux;
52%
toluene-4-sulfonic acid; In xylene; for 3h; Reflux;
52%
at 250 ℃; for 3h;
at 250 ℃; for 3h;
30 g
at 250 ℃; for 3h;
N<SUP>1</SUP>-(4-bromophenyl)benzene -1,2 -diamine
100953-52-4

N1-(4-bromophenyl)benzene -1,2 -diamine

benzaldehyde
100-52-7

benzaldehyde

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene
760212-58-6

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene

Conditions
Conditions Yield
With acetic acid; Reflux;
70%
In 2-methoxy-ethanol; for 12h; Inert atmosphere; Schlenk technique; Reflux;
43%
In water; at 100 ℃;
299 mg
With acetic acid; In 2-ethoxy-ethanol; for 24h; Inert atmosphere; Reflux;
benzaldehyde; With sodium hydrogensulfite; In water; at 20 ℃; for 5h;
N1-(4-bromophenyl)benzene -1,2 -diamine; In ethanol; water; for 24h; Reflux; Inert atmosphere;
4-bromo-aniline
106-40-1

4-bromo-aniline

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene
760212-58-6

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene

Conditions
Conditions Yield
Multi-step reaction with 3 steps
1.1: sodium acetate / 8 h / 180 °C / Inert atmosphere
2.1: sodium dithionite / ethyl acetate; water; tetrahydrofuran / 5 h / 20 °C / Inert atmosphere
2.2: 1 h / 20 °C
3.1: toluene-4-sulfonic acid / xylene / 3 h / Reflux
With sodium dithionite; sodium acetate; toluene-4-sulfonic acid; In tetrahydrofuran; water; ethyl acetate; xylene;
Multi-step reaction with 3 steps
1: water / 2.5 h / 100 °C
2: indium; hydrogenchloride / water / 1 h / 100 °C
3: water / 100 °C
With hydrogenchloride; indium; In water;
Multi-step reaction with 3 steps
1: dimethyl sulfoxide / 48 h / 100 °C / Inert atmosphere; Schlenk technique
2: tin(II) chloride dihdyrate / ethanol / 3 h / Inert atmosphere; Reflux; Schlenk technique
3: 2-methoxy-ethanol / 12 h / Inert atmosphere; Schlenk technique; Reflux
With tin(II) chloride dihdyrate; In ethanol; 2-methoxy-ethanol; dimethyl sulfoxide;
Multi-step reaction with 3 steps
1.1: potassium fluoride dihydrate / 30 h / 170 - 180 °C / Inert atmosphere
2.1: tin(II) chloride dihdyrate / ethanol / 10 h / Inert atmosphere
3.1: 1-methyl-pyrrolidin-2-one / 4 h / 20 - 60 °C
3.2: 3 h / 130 - 250 °C / Inert atmosphere
With 1-methyl-pyrrolidin-2-one; potassium fluoride dihydrate; tin(II) chloride dihdyrate; In ethanol;
Multi-step reaction with 4 steps
1: potassium fluoride / 72 h / 180 °C
2: tin(II) chloride dihdyrate / ethanol / 12 h / 80 °C
3: triethylamine / tetrahydrofuran / 0.5 h / 0 °C
4: toluene-4-sulfonic acid / 5,5-dimethyl-1,3-cyclohexadiene / 12 h / 150 °C
With potassium fluoride; tin(II) chloride dihdyrate; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; ethanol;
Multi-step reaction with 3 steps
1.1: potassium fluoride / 30 h / 170 - 180 °C
2.1: tin(II) chloride dihdyrate / ethanol / 5 h / Reflux
3.1: 1-methyl-pyrrolidin-2-one / 3.5 h / 20 - 50 °C / Inert atmosphere
3.2: 3 h / 250 °C / Inert atmosphere
With potassium fluoride; tin(II) chloride dihdyrate; In 1-methyl-pyrrolidin-2-one; ethanol;
4-bromo-N-(2-nitrophenyl)benzenamine
58476-59-8

4-bromo-N-(2-nitrophenyl)benzenamine

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene
760212-58-6

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1.1: sodium dithionite / ethyl acetate; water; tetrahydrofuran / 5 h / 20 °C / Inert atmosphere
1.2: 1 h / 20 °C
2.1: toluene-4-sulfonic acid / xylene / 3 h / Reflux
With sodium dithionite; toluene-4-sulfonic acid; In tetrahydrofuran; water; ethyl acetate; xylene;
Multi-step reaction with 2 steps
1: indium; hydrogenchloride / water / 1 h / 100 °C
2: water / 100 °C
With hydrogenchloride; indium; In water;
Multi-step reaction with 2 steps
1: tin(II) chloride dihdyrate / ethanol / 3 h / Inert atmosphere; Reflux; Schlenk technique
2: 2-methoxy-ethanol / 12 h / Inert atmosphere; Schlenk technique; Reflux
With tin(II) chloride dihdyrate; In ethanol; 2-methoxy-ethanol;
Multi-step reaction with 2 steps
1.1: tin(II) chloride dihdyrate / ethanol / 10 h / Inert atmosphere
2.1: 1-methyl-pyrrolidin-2-one / 4 h / 20 - 60 °C
2.2: 3 h / 130 - 250 °C / Inert atmosphere
With 1-methyl-pyrrolidin-2-one; tin(II) chloride dihdyrate; In ethanol;
Multi-step reaction with 3 steps
1: tin(II) chloride dihdyrate / ethanol / 12 h / 80 °C
2: triethylamine / tetrahydrofuran / 0.5 h / 0 °C
3: toluene-4-sulfonic acid / 5,5-dimethyl-1,3-cyclohexadiene / 12 h / 150 °C
With tin(II) chloride dihdyrate; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; ethanol;
Multi-step reaction with 2 steps
1.1: tin(II) chloride dihdyrate / ethanol / 5 h / Reflux
2.1: 1-methyl-pyrrolidin-2-one / 3.5 h / 20 - 50 °C / Inert atmosphere
2.2: 3 h / 250 °C / Inert atmosphere
With tin(II) chloride dihdyrate; In 1-methyl-pyrrolidin-2-one; ethanol;
N′-(4-bromophenyl)benzamidine
21719-91-5

N′-(4-bromophenyl)benzamidine

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene
760212-58-6

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene

Conditions
Conditions Yield
With iodine; oxygen; In 1,1,2,2-tetrachloroethane; at 140 ℃; for 24h;
77%
ortho-nitrofluorobenzene
1493-27-2,127723-77-7

ortho-nitrofluorobenzene

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene
760212-58-6

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene

Conditions
Conditions Yield
Multi-step reaction with 3 steps
1: water / 2.5 h / 100 °C
2: indium; hydrogenchloride / water / 1 h / 100 °C
3: water / 100 °C
With hydrogenchloride; indium; In water;
Multi-step reaction with 3 steps
1: dimethyl sulfoxide / 48 h / 100 °C / Inert atmosphere; Schlenk technique
2: tin(II) chloride dihdyrate / ethanol / 3 h / Inert atmosphere; Reflux; Schlenk technique
3: 2-methoxy-ethanol / 12 h / Inert atmosphere; Schlenk technique; Reflux
With tin(II) chloride dihdyrate; In ethanol; 2-methoxy-ethanol; dimethyl sulfoxide;
Multi-step reaction with 3 steps
1.1: potassium fluoride dihydrate / 30 h / 170 - 180 °C / Inert atmosphere
2.1: tin(II) chloride dihdyrate / ethanol / 10 h / Inert atmosphere
3.1: 1-methyl-pyrrolidin-2-one / 4 h / 20 - 60 °C
3.2: 3 h / 130 - 250 °C / Inert atmosphere
With 1-methyl-pyrrolidin-2-one; potassium fluoride dihydrate; tin(II) chloride dihdyrate; In ethanol;
Multi-step reaction with 4 steps
1: potassium fluoride / 72 h / 180 °C
2: tin(II) chloride dihdyrate / ethanol / 12 h / 80 °C
3: triethylamine / tetrahydrofuran / 0.5 h / 0 °C
4: toluene-4-sulfonic acid / 5,5-dimethyl-1,3-cyclohexadiene / 12 h / 150 °C
With potassium fluoride; tin(II) chloride dihdyrate; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; ethanol;
Multi-step reaction with 3 steps
1.1: potassium fluoride / 30 h / 170 - 180 °C
2.1: tin(II) chloride dihdyrate / ethanol / 5 h / Reflux
3.1: 1-methyl-pyrrolidin-2-one / 3.5 h / 20 - 50 °C / Inert atmosphere
3.2: 3 h / 250 °C / Inert atmosphere
With potassium fluoride; tin(II) chloride dihdyrate; In 1-methyl-pyrrolidin-2-one; ethanol;
2-nitrophenyl bromide
577-19-5

2-nitrophenyl bromide

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene
760212-58-6

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene

Conditions
Conditions Yield
Multi-step reaction with 3 steps
1.1: sodium acetate / 8 h / 180 °C / Inert atmosphere
2.1: sodium dithionite / ethyl acetate; water; tetrahydrofuran / 5 h / 20 °C / Inert atmosphere
2.2: 1 h / 20 °C
3.1: toluene-4-sulfonic acid / xylene / 3 h / Reflux
With sodium dithionite; sodium acetate; toluene-4-sulfonic acid; In tetrahydrofuran; water; ethyl acetate; xylene;
N<SUP>1</SUP>-(4-bromophenyl)benzene -1,2 -diamine
100953-52-4

N1-(4-bromophenyl)benzene -1,2 -diamine

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene
760212-58-6

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: triethylamine / tetrahydrofuran / 0.5 h / 0 °C
2: toluene-4-sulfonic acid / 5,5-dimethyl-1,3-cyclohexadiene / 12 h / 150 °C
With toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene;
4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene
760212-58-6

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene

(9,10-diphenylanthracene-2-yl)boronic acid
597553-98-5

(9,10-diphenylanthracene-2-yl)boronic acid

1-[4-(9,10-diphenylanthracen-2-yl)-phenyl]-2-phenyl-1H-benzimidazole

1-[4-(9,10-diphenylanthracen-2-yl)-phenyl]-2-phenyl-1H-benzimidazole

Conditions
Conditions Yield
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0); In 1,2-dimethoxyethane; water; for 8h; Heating / reflux;
90%
4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene
760212-58-6

4-(2-phenyl-1H-benzo[d]imidazol-1-yl)1-bromobenzene

bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

2-phenyl-1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1H-benzo[d]imidazole
1169709-19-6

2-phenyl-1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1H-benzo[d]imidazole

Conditions
Conditions Yield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 12h;
96%
With tetrakis(triphenylphosphine) palladium(0); potassium acetate; In 1,4-dioxane; at 110 ℃; for 24h;
78%
With tetrakis(triphenylphosphine) palladium(0); potassium acetate; In 1,4-dioxane; at 110 ℃; for 12h; Inert atmosphere;
78%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In tetrahydrofuran; at 85 ℃; for 12h; Inert atmosphere;
76%
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 4h; Inert atmosphere;
72.7%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 80 ℃; for 12h; Inert atmosphere; Schlenk technique;
43%
With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In N,N-dimethyl-formamide; at 80 ℃; for 3h; Inert atmosphere;
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In N,N-dimethyl-formamide; at 120 - 150 ℃; for 10h; Inert atmosphere;
With tetrakis(triphenylphosphine) palladium(0); potassium acetate; In 1,4-dioxane; at 110 ℃; for 24h; Inert atmosphere;
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; for 24h; Inert atmosphere; Reflux;
745 mg
With tetrakis(triphenylphosphine) palladium(0); potassium acetate; In 1,4-dioxane; at 110 ℃; for 24h; Inert atmosphere;

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