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Diethyleneglycolmonohexylether
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Name

Diethyleneglycolmonohexylether

 EINECS 203-988-3
CAS No. 112-59-4 Density 0.933 g/cm3
PSA 38.69000 LogP 1.59220
Solubility Soluble in water. Melting Point ?40 ºC(lit.)
Formula C10H22 O3 Boiling Point 260 ºC at 760 mmHg
Molecular Weight 190.283 Flash Point 140 ºC
Transport Information N/A Appearance N/A
Safety Moderately toxic by skin contact route. Mildly toxic by ingestion. An eye and severe skin irritant. Combustible when exposed to heat or flame; can react with oxidizing materials. To fight fire, use foam, CO2, dry chemical. When heated to decomposition it emits acrid smoke and fumes. See also GLYCOL ETHERS. Risk Codes 21-41
Molecular Structure Molecular Structure of 112-59-4 (2-(2-HEXYLOXYETHOXY)ETHANOL) Hazard Symbols HarmfulXn
Synonyms

2-[2-(Hexyloxy)ethoxy]ethanol;3,6-Dioxa-1-dodecanol; DEGHE; Diethylene glycol hexyl ether; Diethylene glycolmonohexyl ether; HEDG; Hexyl Carbitol; Kyowanol HX 20; NSC 403666; Ucar FilmerEHC; n-Hexoxyethoxyethanol

Article Data 6

Diethyleneglycolmonohexylether Synthetic route

111-25-1

1-bromo-hexane

111-46-6

diethylene glycol

112-59-4

diethylene glycol monohexyl ether

Conditions
ConditionsYield
With potassium hydroxide In 1,4-dioxane at 100 - 105℃;68%
With sodium hydride
75-21-8

oxirane

112-25-4

2-hexyloxyethanol

112-59-4

diethylene glycol monohexyl ether

Conditions
ConditionsYield
With borontrifluoride acetic acid
75-21-8

oxirane

111-27-3

hexan-1-ol

112-59-4

diethylene glycol monohexyl ether

Conditions
ConditionsYield
With boron trifluoride diethyl etherate at 50℃;
111-25-1

1-bromo-hexane

sodium diethylene glycolate

sodium diethylene glycolate

112-59-4

diethylene glycol monohexyl ether

Conditions
ConditionsYield
With diethylene glycol at 200℃;
112-59-4

diethylene glycol monohexyl ether

98-59-9

p-toluenesulfonyl chloride

187748-60-3

2-(2'-n-hexyloxyethoxy)ethyl p-toluenesulfonate

Conditions
ConditionsYield
Stage #1: diethylene glycol monohexyl ether; p-toluenesulfonyl chloride With dmap In dichloromethane at 20℃; for 0.166667h;
Stage #2: With triethylamine In dichloromethane at 20℃; for 3.25h;		100%
With triethylamine In dichloromethane at 0 - 20℃; for 18h; Inert atmosphere;92%
With pyridine In dichloromethane at 20℃; for 3h;71%
With dmap; triethylamine In dichloromethane for 3h;
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

112-59-4

diethylene glycol monohexyl ether

C24H48O6

Conditions
ConditionsYield
Stage #1: diethylene glycol monohexyl ether With sodium hydride In tetrahydrofuran; mineral oil at 20℃; for 0.333333h; Inert atmosphere;
Stage #2: 2-chloromethyl-3-chloroprop-1-ene In tetrahydrofuran; mineral oil at 65℃; for 5.5h; Inert atmosphere;		88%
112-59-4

diethylene glycol monohexyl ether

615-42-9

1,2-Diiodobenzene

1,2-bis-(2-(2-(hexyloxy)ethoxy)ethoxy)benzene

Conditions
ConditionsYield
With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate In 5,5-dimethyl-1,3-cyclohexadiene at 140℃; for 72h; Inert atmosphere;85%
With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate In 5,5-dimethyl-1,3-cyclohexadiene at 140℃; for 72h; Inert atmosphere;85%
112-59-4

diethylene glycol monohexyl ether

72510-64-6

1-[2-(2-chloroethoxy)ethoxy]hexane

Conditions
ConditionsYield
With pyridine; thionyl chloride In toluene at -5 - 100℃; for 2h;84%
With pyridine; thionyl chloride
112-59-4

diethylene glycol monohexyl ether

626-00-6

1,3-Diiodobenzene

1,3-bis(2-(2-hexylethoxy)ethoxy)benzene

Conditions
ConditionsYield
With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate In 5,5-dimethyl-1,3-cyclohexadiene for 20h; Reflux; Inert atmosphere;82%
591-50-4

iodobenzene

112-59-4

diethylene glycol monohexyl ether

928346-61-6

(2-(2-(hexyloxy)ethoxy)ethoxy)benzene

Conditions
ConditionsYield
With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate In 5,5-dimethyl-1,3-cyclohexadiene at 120℃; for 24h; Inert atmosphere;77%
With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate In 5,5-dimethyl-1,3-cyclohexadiene at 120℃; for 24h; Inert atmosphere;77%

Diethyleneglycolmonohexylether Chemical Properties

SYNONYMS Diethylene glycol hexyl ether; 2-((2-Hexyloxy)ethoxy)ethanol; 
Diethylene glycol mono(n-hexyl) ether; Hexol carbitol; Diethylene glycol monohexyl ether; n-Hexoxyethoxyethanol; Diethyleneglycolmonohexylether; 2-((2-Hexyloxy)ethoxy)ethanol; 2-(2-(hexyloxy)ethoxy)ethanol; 
EINECS NO.:203-988-3
FORMULA:CH3(CH2)5OCH2CH2OH
MOL WT:146.23
PHYSICAL STATE:clear liquid
MELTING POINT:-40 °C
BOILING POINT:260 °C
SPECIFIC GRAVITY:0.93 - 0.94
FLASH POINT:141°C
REFRACTIVE INDEX:1.435
SOLUBILITY IN WATER:1.7 (g/100g)

Diethyleneglycolmonohexylether,it is sable under ordinary conditions.

Diethyleneglycolmonohexylether Toxicity Data With Reference

1.   

skn-rbt 10 mg/24H open MLD

   AMIHBC    AMA Archives of Industrial Hygiene and Occupational Medicine. 4 (1951),119.
2.   

skn-rbt 500 mg/24H SEV

   JPETAB    Journal of Pharmacology and Experimental Therapeutics. 82 (1944),377.
3.   

skn-rbt 500 mg open MLD

   UCDS**    Union Carbide Data Sheet. (Industrial Medicine and Toxicology Dept., Union Carbide Corp., 270 Park Ave., New York, NY 10017) 11/3 ,1971.
4.   

eye-rbt 5 mg MOD

   UCDS**    Union Carbide Data Sheet. (Industrial Medicine and Toxicology Dept., Union Carbide Corp., 270 Park Ave., New York, NY 10017) 11/3 ,1971.
5.   

orl-rat LD50:4920 mg/kg

   AMIHBC    AMA Archives of Industrial Hygiene and Occupational Medicine. 4 (1951),119.
6.   

skn-rbt LD50:1500 mg/kg

   AMIHBC    AMA Archives of Industrial Hygiene and Occupational Medicine. 4 (1951),119.

Diethyleneglycolmonohexylether Consensus Reports

n-HEXYL CARBITOL is reported in PA TSCA Inventory. Glycol ether compounds are on the Community Right-To-Know List.

Diethyleneglycolmonohexylether Safety Profile

Moderately toxic by skin contact route. Mildly toxic by ingestion. An eye and severe skin irritant. Combustible when exposed to heat or flame; can react with oxidizing materials. To fight fire, use foam, CO2, dry chemical. When heated to decomposition it emits acrid smoke and fumes. See also GLYCOL ETHERS.

Diethyleneglycolmonohexylether's Risk Statements:21:Harmful in contact with skin;41:Risk of serious damage to eyes   
Diethyleneglycolmonohexylether's Safety Statements:26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice;36/37:Wear suitable protective clothing and gloves;46:If swallowed, seek medical advice immediately and show this container or label;24/25:Avoid contact with skin and eyes
Hazard Codes:Xn
WGK Germany:1

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