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Cas Database |
| Name |
Ethyl 3-(pyridin-2-ylamino)propanoate |
EINECS | -0 |
| CAS No. | 103041-38-9 | Density | 1.132 g/cm3 |
| PSA | 51.22000 | LogP | 1.51970 |
| Solubility | N/A | Melting Point |
48-50°C |
| Formula | C10H14N2O2 | Boiling Point | 337.812 °C at 760 mmHg |
| Molecular Weight | 194.233 | Flash Point | 158.103 °C |
| Transport Information | N/A | Appearance | off-white crystals |
| Safety | Risk Codes | N/A | |
| Molecular Structure |
|
Hazard Symbols | N/A |
| Synonyms |
b-Alanine, N-2-pyridyl-, ethylester (6CI); |
Article Data | 11 |
Ethyl 3-(pyridin-2-ylamino)propanoate Synthetic route
- 504-29-0
2-aminopyridine
- 140-88-5
ethyl acrylate
- 103041-38-9
2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate
| Conditions | Yield |
|---|---|
| With trifluorormethanesulfonic acid In ethanol at 120℃; for 12h; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; Green chemistry; chemoselective reaction; | 94% |
| With acetic acid In acetic acid at 88℃; Product distribution / selectivity; | 86.7% |
| In acetic acid at 88℃; Product distribution / selectivity; | 86.7% |
- 64-17-5
ethanol
- 104961-64-0
3-[(pyridin-2-yl)amino]propanoic acid
- 103041-38-9
2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate
| Conditions | Yield |
|---|---|
| With thionyl chloride at 0 - 70℃; for 12h; | 69.2% |
- 504-29-0
2-aminopyridine
- 98-29-3
4-tert-Butylcatechol
- 140-88-5
ethyl acrylate
A
- 103041-38-9
2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate
B
- 5439-14-5
3,4-dihydro-pyrido[1,2-a]pyrimidin-2-one
- 504-29-0
2-aminopyridine
- 140-88-5
ethyl acrylate
A
- 103041-38-9
2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate
B
- 5439-14-5
3,4-dihydro-pyrido[1,2-a]pyrimidin-2-one
- 103041-38-9
2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate
| Conditions | Yield |
|---|---|
| With triethylamine In ethyl acetate at -10℃; Reagent/catalyst; Temperature; Solvent; | 97.7% |
- 103041-38-9
2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate
- 99548-53-5
3-Bromo-4-ethylbenzoic acid
| Conditions | Yield |
|---|---|
| Stage #1: 3-Bromo-4-ethylbenzoic acid With thionyl chloride In tetrahydrofuran; N,N-dimethyl-formamide at -20 - 20℃; for 5h; Stage #2: 2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate With pyridine In tetrahydrofuran; N,N-dimethyl-formamide at 20℃; for 6h; Solvent; Reagent/catalyst; | 97% |
- 103041-38-9
2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate
- 41263-74-5
4-(methylamino)-3-nitrobenzoic acid
- 1187067-68-0
ethyl 3-[[4-(methylamino)-3-nitrobenzoyl](pyridin-2-yl)amino]propanoate hydrochloride
| Conditions | Yield |
|---|---|
| With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 18h; Solvent; Reagent/catalyst; | 95.2% |
- 103041-38-9
2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate
- 38818-50-7
4-chloro-3-nitro-benzoyl chloride
- 1620205-04-0
3-[(4-chloro-3-nitrobenzoyl)pyridin-2-yl-amino]propionic acid ethyl ester
| Conditions | Yield |
|---|---|
| With triethylamine In dichloromethane at 20℃; for 1h; Solvent; Reagent/catalyst; | 87% |
| With N-ethyl-N,N-diisopropylamine In dichloromethane at -5 - 0℃; for 1h; | |
| With triethylamine In dichloromethane at 20℃; for 1h; Solvent; Reagent/catalyst; | 16.3 g |
- 103041-38-9
2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate
| Conditions | Yield |
|---|---|
| Stage #1: 2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate; 4-methylamino-3-nitrobenzoyl chloride hydrochloride With triethylamine In toluene at 0 - 30℃; for 3h; Large scale; Stage #2: In ethanol; toluene at 20 - 70℃; Large scale; | 87% |
- 103041-38-9
2-chloromethyl-1-methyl-1H-benzimidazole-5 ethyl acetate
- 1307233-94-8
N-[[2-(chloromethyl)-1-methyl-1H-benzimidazol-5-yl]carbonyl]-N-2-pyridyl-β-alanine ethyl ester
| Conditions | Yield |
|---|---|
| In ethyl acetate at 20℃; for 1h; | 85% |
Ethyl 3-(pyridin-2-ylamino)propanoate Chemical Properties
Product Name: Ethyl 3-(pyridin-2-ylamino)propanoate (CAS NO.103041-38-9)
Molecular Formula: C10H14N2O2
Molecular Weight: 194.23g/mol
Mol File: 103041-38-9.mol
Boiling point: 337.812 °C at 760 mmHg
Flash Point: 158.103 °C
Density: 1.132 g/cm3
Index of Refraction: 1.545
Molar Refractivity: 54.26 cm3
Molar Volume: 171.623 cm3
Surface Tension: 44.869 dyne/cm
Enthalpy of Vaporization: 58.11 kJ/mol
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