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Ethylbutylamine

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Name

Ethylbutylamine

EINECS 236-415-0
CAS No. 13360-63-9 Density 0.74
PSA 12.03000 LogP 1.78690
Solubility partly soluble Melting Point -77.8oC
Formula C6H15 N Boiling Point 108 ºC
Molecular Weight 101.192 Flash Point 18 ºC
Transport Information UN 2733 Appearance A colorless liquid with an ammonia-like odor.
Safety A poison by ingestion. When heated to decomposition it emits toxic vapors of NOx. Risk Codes R11;R22;R34   
Molecular Structure Molecular Structure of 13360-63-9 (Ethylbutylamine) Hazard Symbols
Synonyms

Butylamine,N-ethyl- (6CI,7CI,8CI); Butylethylamine; Ethylbutylamine; N-Butyl-N-ethylamine;N-Butylethylamine; N-Ethyl-1-butanamine; N-Ethyl-N-butylamine;N-Ethylbutanamine; N-Ethylbutylamine

Article Data 38

Ethylbutylamine Synthetic route

(4-{tris[2-(perfluorohexyl)ethyl]silyl}benzyl) (butyl)(ethyl)carbamate

13360-63-9

N-ethylbutylamine

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In methanol at 20℃; for 16h;80%
122-56-5

tributyl borane

81375-29-3

O-(p-toluenesulfonyl)-N-ethylhydroxylamine

13360-63-9

N-ethylbutylamine

Conditions
ConditionsYield
In tetrahydrofuran for 2h; Ambient temperature;77%
917-54-4

methyllithium

33704-65-3

Butyl-phenylsulfanylmethyl-amine; hydrochloride

13360-63-9

N-ethylbutylamine

Conditions
ConditionsYield
In diethyl ether at -60℃;76%
75-04-7

ethylamine

109-73-9

N-butylamine

A

102-82-9

tributyl-amine

B

13360-63-9

N-ethylbutylamine

C

4444-68-2

N,N-diethylbutylamine

D

4458-33-7

di-n-butylethylamine

E

111-92-2

dibutylamine

F

109-89-7

diethylamine

G

121-44-8

triethylamine

Conditions
ConditionsYield
With hydrogen at 200℃; under 6000.6 Torr; Reagent/catalyst; Temperature;A n/a
B 60.7%
C n/a
D n/a
E n/a
F n/a
G n/a
75-04-7

ethylamine

71-36-3

butan-1-ol

13360-63-9

N-ethylbutylamine

Conditions
ConditionsYield
With hydrogen at 150℃; under 3750.38 Torr; for 8h; Temperature; Pressure; Reagent/catalyst;55.3%
With hydrogen; nickel at 150℃;
109-74-0

propyl cyanide

64-17-5

ethanol

A

13360-63-9

N-ethylbutylamine

B

4853-56-9

(butylidene)butylamine

C

109-73-9

N-butylamine

Conditions
ConditionsYield
With Co(9.8%)/SiO2 catalyst; hydrogen at 129.84℃; under 9750.98 Torr; Reagent/catalyst; Temperature;A 30.5%
B 25.6%
C 42.3%
14925-83-8

N,N-dichloro-n-butylamine

557-20-0

diethylzinc

A

13360-63-9

N-ethylbutylamine

B

109-73-9

N-butylamine

Conditions
ConditionsYield
With Petroleum ether
1611-12-7

ethyl-butyliden-amine

13360-63-9

N-ethylbutylamine

Conditions
ConditionsYield
With nickel; Petroleum ether at 75℃; under 154457 Torr; Hydrogenation;
With ethanol; sodium
With ethanol; platinum Hydrogenation;
77228-69-4

N-benzyl-N-ethylbutan-1-amine

13360-63-9

N-ethylbutylamine

Conditions
ConditionsYield
With platinum(IV) oxide; acetic acid at 65 - 75℃; Hydrogenolyse;
75-04-7

ethylamine

123-72-8

butyraldehyde

13360-63-9

N-ethylbutylamine

Conditions
ConditionsYield
With ethanol; platinum Hydrogenation;
(i), (ii) H2, Pd-C, EtOH; Multistep reaction;
With potassium hydroxide; dipotassium hydrogenphosphate; phosphoric acid at 10 - 12℃; for 4h; electrochemical reductive amination, lead cathode, current density 0.05 A/cm2, pH 12; Yield given;

Ethylbutylamine Chemical Properties

  The molecular formula of N-ETHYLBUTYLAMINE(13360-63-9) is C6H15N and its formula weight is 101.19g/mol.Its EINECS is 236-415-0.Its liansport information is UN 2733.The appearance of N-ETHYLBUTYLAMINE(13360-63-9) is colorless liquid.The density of ) is 0.74 g/mL at 25 °C(lit.).The boiling point is 108 °C(lit.).The refractive index is about n20/D 1.405(lit.) and molar refractivity is 33.44 cm3.Its fiash point is 18.3 °C and the vapor pressenge is 18 mm Hg ( 20 °C).Its enthalpy of vaporization is 33.97 kJ/mol.Surface Tension is 23 dyne/cm.N-ETHYLBUTYLAMINE(13360-63-90) has the property of being soluble in alcohol, ether and other organic solvents,partly dissolved in water.                                                         
    The chemical synonyms of are 1-Butanamine,N-ethyl-;butyl(ethyl)amine;Butylamine, N-ethyl-;Butylamine,N-ethyl-;Butylethylamine;N-Butylethylamine;N-Butyl-N-ethylamine;n-ethyl-1-butanamin .Its product categories is Amines;C2 to C6 and Nitrogen Compounds.The molecular structure of N-ETHYLBUTYLAMINE(13360-63-9) is .

Ethylbutylamine Uses

N-ETHYLBUTYLAMINE(13360-63-9) can be used as intermediate of  herbicide .

Ethylbutylamine Production

Its preparation method is that alcohol and ammonia react with ethanol  in the deoxidation and the presence of hydrogenation catalyst in the 170 ~ 210 ℃ / 1013 kPa , at the same time aminating and aminating derived products.

Ethylbutylamine Toxicity Data With Reference

1.   

orl-rat LD50:310 mg/kg

   GISAAA    Gigiena i Sanitariya. 39 (3)(1974),106.
2.   

orl-mus LD50:418 mg/kg

   GISAAA    Gigiena i Sanitariya. 39 (3)(1974),106.

Ethylbutylamine Consensus Reports

Reported in EPA TSCA Inventory.

Ethylbutylamine Safety Profile

A poison by ingestion. When heated to decomposition it emits toxic vapors of NOx.                                                           Risk Codes:R11;R22;R34
Hazard codes  is    F,  C .
Risk statements is 11-22-34 and safety statements  is 16-26-36/37/39-45-33.
HazardClass is  3.

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