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COMMUNICATION
Chemical Communications
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200 mesh, ~3.0 mmol/g loading, 2% cross-linked with
divinylbenzene. For 4a, 2 g of TPP-resin was used; for other flow
setups, 1 g TPP-resin was used.
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15. In the flow settings, 120 °C was used instead of 150 °C to
maintain the endurance of the system while achieving
comparable results. See the Supporting Information for more
details.
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16. We could not obtain a solid state 31P NMR spectrum for the
polymer-bound phosphonium ylide intermediate due to the
unstable nature of this species.
10. See Supporting Information for more details.
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