Journal of Organometallic Chemistry p. 399 - 408 (1984)
Update date:2022-08-29
Topics:
Berlan, J.
Besace, Y.
Prat, D.
Pourcelot, G.
Addition of lithium dimethylcuprate to the chiral oxazolidine (1) in ether or in hexane leads to 3-phenylbutanals having the S or R configuration, respectively, with high optical yield in the latter case (e.e. = ca. 80percent).The 1H NMR study of the intermediate oxazolidine allows accurate determination of the optical yield and could be applied to the determination of the absolute configuration and optical purity of other 3-arylalkanals.
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