Bulletin of the Chemical Society of Japan p. 965 - 966 (1983)
Update date:2022-08-24
Topics:
Cracknell, Mark Edward
Goodland, Michael Charles
McOmie, John Frederick William
Four mono(arylhydrazone)s of benzocyclobutene-1,2-dione (BBD) have been prepared in which the aryl group is 2,4-dinitrophenyl, 4-bromophenyl, phenyl, and 4-nitrophenyl.The first three have been separated into their E- nd Z-isomers whose configurations are assigned on the basis of spectra and Rf values.Improvements in the preparation of BBD from 1,2-dibromo-1,2-dihydrobenzocyclobutene are described.
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