Recueil des Travaux Chimiques des Pays-Bas p. 376 - 383 (1993)
Update date:2022-08-11
Topics:
Barf, Tjeerd
Jansen, Johan F. G. A.
Bolhuis, Fre van
Spek, Anthony L.
Feringa, Ben L.
Bulky ligands for cleft-type metal complexes were synthesized from thioketones and diamines in yields varying from 20 - 80 percent.A molecular structure determination of one ligand, N,N'-bis(12H-benzoxanthen-12-ylidene)-1,2-propanediamine (19), was performed.A metallo-cleft was constructed by a self-assembling process with zinc(II) chloride.A crystallographic study of this zinc complex (24) revealed surprisingly that an anti-syn inversion of the imine moieties of the ligand had taken place during complexation.
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