Tetrahedron Letters p. 4665 - 4668 (1995)
Update date:2022-08-28
Topics:
Gentilucci, Luca
Grijzen, Yvonne
Thijs, Lambertus
Zwanenburg, Binne
The synthesis of optically active 2H-azirine-2-carboxylic esters was achieved by Swern oxidation of the corresponding aziridine-carboxylic esters. For both trans and cis aziridine esters this oxidation gives a regioselective introduction of the double bond which is not in conjugation with the ester function. The methyl ester of ent-Azirinomycin was prepared in this manner.
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