Tetrahedron p. 6111 - 6122 (1998)
Update date:2022-08-10
Topics:
Caballero, Esther
Medarde, Manuel
De Clairac, Rafael Pelaez-Lamamie
Sahagun, Heidi
Tome, Fernando
The synthesis of the first representative compound of 7-aryl anthracycline analogues, is described. 1-Alkyl-3-trialkylsiloxydienes, prepared from readily available materials, are transformed through a Diels- Alder cycloaddition into a tetracyclic ketone, that is converted into (±)- 7-(3,4,5-trimethoxyphenyl)-7-deoxyidarubicinone. The conformations of the target compound and intermediate products are studied.
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