SYNTHESIS AND NMR SPECTRA OF 2,2,2,-TRIDEUTERIOETHYLARSINE AND 2,2,2-TRIDEUTERIOETHYLCYCLOPENTAARSINE

DOI: 10.1016/S0022-328X(00)81950-6

Source and publish data:

Journal of Organometallic Chemistry p. 119 - 124 (1982)

Update date:2022-08-17

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Authors:

Rheingold, A. L.

Natarajan, S.

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Article abstract of DOI:10.1016/S0022-328X(00)81950-6

Pentakis(2,2,2-trideuterioethyl)cyclopentaarsine (PDECA) was synthesized by the reaction of 2,2,2-trideuterioethylarsine with dibenzylmercury.Variable temperature NMR spectra in C6D6 are interpreted in terms of fast pseudorotation.NMR and mass spectra and synthesis of 2,2,2-trideuterioethylarsine are also described.

Full text of DOI:10.1016/S0022-328X(00)81950-6

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